2,3,6,7,10,11-HEXABROMOTRIPHENYLENE
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2,3,6,7,10,11-HEXABROMOTRIPHENYLENE
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CAS No:
82632-80-2
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Formula:
C18H6Br6
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Chemical Name:
2,3,6,7,10,11-HEXABROMOTRIPHENYLENE
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Synonyms:
2,3,6,7,10,11-hexabromotriphenylene;Triphenylene, 2,3,6,7,10,11-hexabromo-;ACMC-209ppl;SCHEMBL311663;CTK3D8135;DTXSID60454505;KS-000014JU;ABP001040;ANW-37591;AKOS015835444
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CAS No:
Safety Information
P264, P280, P302+P352, P305+P351+P338, P321, P332+P313, P337+P313, P362
H315
|Warning|H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]|P264, P280, P302+P352, P305+P351+P338, P321, P332+P313, P337+P313, and P362|The GHS information provided by 1 company from 1 notification to the ECHA C&L Inventory.
2,3,6,7,10,11-HEXABROMOTRIPHENYLENE Use and Manufacturing
Under nitrogen, bromine (9.0 mL, 349 mmol) was added dropwise to 9 (3.95 g, 17.3 mmol) and Fe (410 mg, 7.34 mmol) in nitrobenzene (200 mL) with stirring at rt for 20 min and furthermore at 210 °C for 3 h. After cooling the reaction mixture to room temperature, Et5.0 g of triphenylene, 0.49 g of iron powder and 10.1 ml of bromine were added to a reaction vessel purged with nitrogen and heated, followed by stirring at 170 ° C. for 10 hours. After cooling to room temperature, 100 ml of tetrahydrofuran was added and the mixture was further stirred for 0.5 hour. Filtration gave 2, 3, 6, 7, 10, 11-hexabromotriphenylene gray powder13.5 g (yield 84percent) was obtained.Step a) [0222] Triphenylene (1 equivalent) is brominated with 8 equivalents of Br
Computed Properties
Molecular Weight:701.7
XLogP3:9
Exact Mass:701.55083
Monoisotopic Mass:695.55698
Heavy Atom Count:24
Complexity:364
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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2,3,6,7,10,11-HEXABROMOTRIPHENYLENE
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