2-Methyl-5-pyrimidinemethanol
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2-Methyl-5-pyrimidinemethanol
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CAS No:
2239-83-0
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Formula:
C6H8N2O
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Chemical Name:
2-Methyl-5-pyrimidinemethanol
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Synonyms:
2-Methyl-5-pyrimidinemethanol;(2-Methylpyrimidin-5-yl)methanol;SCHEMBL2171192;5-Pyrimidinemethanol,2-methyl-;CTK4E9382;DTXSID70562988;ACT08652;(2-Methyl-pyrimidin-5-yl)-methanol;ANW-48717;MFCD09414732
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CAS No:
Characteristics
46
-0.3
white crystalline solid
1.171
102-103°C
237°C
97.1±20.4 °C
1.549
0.0253mmHg at 25°C
2-Methyl-5-pyrimidinemethanol Use and Manufacturing
To a mixture of 2-methylpyrimidine-5-carbaldehyde (8 g, 66 mmol, compound 44b) in MeOH (100 mL) was added NaBHA solution of 2-methyl-pyrimidine-5-carbaldehyde (5 g, 41 mmol) in MeOH (100 mL) was added NaBHStep 1 (2-methylpyrimidin-5-yl)methanol To a solution of 2-methylpyrimidine-5-carboxylic acid (150 mg, 1.23 mmOl) in ethanol (5 mL) was added sodium borohydride(93 mg, 2.46 mmol). The mixture was stirred at room temperature for 3 h. It was quenched with aqueous HC1 (2 N, 2 mL), extracted with DCM, dried over sodium sulfate, filtered and concentrated give the yellow oil product (2-methylpyrimidin-5-yl)methanol (95 mg, 62.6percent). LCMS MHTo a solution of 2-methylpyrimidine-5-carboxylic acid (150 mg, 1.23 mml) in ethanol (5 mL) was added sodium borohydride (93 mg, 2.46 mmol).
Computed Properties
Molecular Weight:124.14
XLogP3:-0.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:124.063662883
Monoisotopic Mass:124.063662883
Topological Polar Surface Area:46
Heavy Atom Count:9
Complexity:79.1
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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