6-Methyl-1H-benzimidazole-2-methanol
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6-Methyl-1H-benzimidazole-2-methanol
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CAS No:
20034-02-0
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Formula:
C9H10N2O
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Chemical Name:
6-Methyl-1H-benzimidazole-2-methanol
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Synonyms:
1H-Benzimidazole-2-methanol,6-methyl-;2-Benzimidazolemethanol,5-methyl-;1H-Benzimidazole-2-methanol,5-methyl-;2-Benzimidazolemethanol,5(or 6)-methyl-;6-Methyl-1H-benzimidazole-2-methanol;(5-Methyl-1H-benzimidazol-2-yl)methanol;(6-Methyl-1H-1,3-benzodiazol-2-yl)methanol;(5-Methyl-1H-1,3-benzodiazol-2-yl)methanol;(6-Methyl-1H-benzimidazol-2-yl)methanol
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CAS No:
Safety Information
26-39
Xi: Irritant;
|Warning|H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]|P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, and P501|The GHS information provided by 1 company from 1 notification to the ECHA C&L Inventory.
6-Methyl-1H-benzimidazole-2-methanol Use and Manufacturing
(5-Methyl-1H-benzimidazole-2-yl)-methanol 25 was prepared using the Phillips procedure [1], 4-Methyl-1, 2-phenylenediamine (12.22 g; 0.1 mol) and glycolic acid (11.40 g; 0.15 mmol) in hydrochloric acid (50 ml, 5.5 M) were heated under reflux with for 3 h. The reaction mixture was cooled to room temperature and ammonia solution was added and the mixture cooled in ice until a bright brown precipitate formed. The resulting solid was recrystallised from aqueous ethanol to give (5-methyl-1H-benzimidazole-2-yl)-methanol as a pale creamy powdery solid Yield 100percent.General procedure: To a mixture of 1a–1c (10 mmol) with glycolic acid (2.28 g, 30 mmol) was added concentrated H3PO4(20 mL). The reaction mixture was refluxed at 130°C for 3 h, then quenched with 20percent NaOH. The respective solid product was collected by filtration.Step 1
Computed Properties
Molecular Weight:162.19
XLogP3:1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:162.079312947
Monoisotopic Mass:162.079312947
Topological Polar Surface Area:48.9
Heavy Atom Count:12
Complexity:163
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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6-Methyl-1H-benzimidazole-2-methanol
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