H-VAL-NH2HCL
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H-VAL-NH2HCL
structure -
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CAS No:
3014-80-0
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Formula:
C5H13ClN2O
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Chemical Name:
H-VAL-NH2HCL
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Synonyms:
VAL-NH2.HCL; H-VAL-NH2HCL; VALINE-NH2HC; VALINE-NH2HCL; H-L-VAL-NH2HCL; H-VAL-NH2• L-ValinamideHCL; L-ValineamideHCL; L-ValineamideHCL98+%
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CAS No:
Characteristics
69.11000
266-270ºC(lit.)
273.6ºC at 760 mmHg
119.3ºC
27 ° (C=1, H2O)
soluble in methanol (50 mg/ ml-clear, colorless solution).
-20ºC
H-VAL-NH2HCL Use and Manufacturing
General procedure: The appropriate carboxylic acid (1.0 mmol), appropriate amine (1.2 eq.), hydroxybenzotriazole (203 mg, 1.5 eq., 1.5 mmol), 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride (288 mg, 1.5 eq., 1.5 mmol) and N, N-diisopropylethylamine (871 muL, 5 eq., 5.0 mmol) were dissolved in N, N-dimethylformamide (5 mL) and the mixture stirred for 24 h. The reaction mixture was diluted with saturated aqueous sodium hydrogen carbonate (30 mL), extracted with ethyl acetate (3 × 20 mL), washed with saturated aqueous sodium hydrogen carbonate (30 mL), saturated aqueous ammonium chloride (30 mL) and aqueous lithium chloride (1 M, 30 mL), dried over anhydrous magnesium sulfate and concentrated under reduced pressure.
L-Valine Amide is a reagent used in the synthesis of alkylpyrazines. Also used in the synthesis of elastase inhibitory activity.
Computed Properties
Molecular Weight:152.62
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:152.0716407
Monoisotopic Mass:152.0716407
Topological Polar Surface Area:69.1
Heavy Atom Count:9
Complexity:90.4
Defined Atom Stereocenter Count:1
Covalently-Bonded Unit Count:2
Compound Is Canonicalized:Yes
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