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1,3-Dichloro-5-iodobenzene

1,3-Dichloro-5-iodobenzene structure

CAS No:
3032-81-3
Formula:
C6H3Cl2I
Chemical Name:
1,3-Dichloro-5-iodobenzene
Synonyms:
Benzene,1,3-dichloro-5-iodo-;1,3-Dichloro-5-iodobenzene;3,5-Dichlorophenyl iodide;3,5-Dichloroiodobenzene;1-Iodo-3,5-dichlorobenzene;NSC 80149;3,5-Dichloro-1-iodobenzene
Categories:
Organic Chemistry > Hydrocarbons and Derivatives

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Description

Pale yellow to pale orange crystals or powder

1,3-Dichloro-5-iodobenzene Basic Attributes

Molecular Weight：

272.9

Exact Mass：

272.90

BRN：

2242455

EC Number：

221-216-3

UNII：

V7B3N2933K

NSC Number：

80149

DSSTox ID：

DTXSID4062800

HScode：

29039990

Characteristics

PSA：

XLogP3：

3.8

Appearance：

tan - off-white powder.

Density：

2.0±0.1 g/cm3

Melting Point：

54 °C

Boiling Point：

127°C20mm

Flash Point：

127°C/20mm

Refractive Index：

1.643

Storage Conditions：

Store in a tightly closed container. Store in a cool, dry, well-ventilated area away from incompatible substances.

Safety Information

Transport codes：

NONH for all modes of transport

wgk germany：

hazard class code：

36/37/38

safety instructions：

24/25

Marks：

Hazard note：

Irritant

Stability/Shelf Life：

Stable at room temperature in closed containers under normal storage and handling conditions.

Precautionary statement(s)：

P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, P501

Hazard Statements：

H315

GHS Classification：

|Warning|H302 (22.22%): Harmful if swallowed [Warning Acute toxicity, oral]|P261, P264, P270, P271, P280, P301+P312, P302+P352, P304+P312, P304+P340, P305+P351+P338, P312, P321, P322, P330, P332+P313, P337+P313, P362, P363, P403+P233, P405, and P501|Aggregated GHS information provided by 9 companies from 5 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.

1,3-Dichloro-5-iodobenzene Use and Manufacturing

Methods of Manufacturing

8-Mercaptoadenine (3.6 mmol), neocuproine hydrate (0.36 mmol), Cul (0.36 mmol), NaO-?-Bu (7.2 mmol), 3, 5-dichloro-iodobenzene (10.8 mmol), and anhydrous DMF (24 mL) were added to a round bottom flask flushed with nitrogen. The flask was sealed with Teflon tape and heated at 1 10 °C with stirring for 24-36 h under nitrogen. Solvent was removed under reduced pressure and the resulting residue was chromatographed (CH2Cl2:MeOH:AcOH, 20: 1 :0.5) to yield 15 as a yellow solid in 44 percent yield. -NMR (400 MHz, DMSO-i/6) delta 13.49 (IH, br s), 8.13 (IH, s), 7.59 (IH, s), 7.47 (2H, s), 7.36 (2H, br s); MS (ESI): m/z 312.1 [M + H+].

Manufacturing Info：

Benzene, 1,3-dichloro-5-iodo-: INACTIVE

Computed Properties

Molecular Weight:272.89
XLogP3:3.8
Exact Mass:271.86565
Monoisotopic Mass:271.86565
Heavy Atom Count:9
Complexity:87.1
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

Recommended Suppliers of 1,3-Dichloro-5-iodobenzene

HANGZHOU LEAP CHEM CO., LTD. Contact Supplier

CN
5 YRS

Business licensed

Trader Supplier of Intermediates,Building blocks,API,Silicones,Peptides,Lab chemicals,Biochemicals,Pharmaceuticals,Screening Compounds,Food Additives

3,5-Dichloroiodobenzene

CAS No.: 3032-81-3

Content: 99.00%

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Hangzhou KieRay Chem Co.,LTD Contact Supplier

CN
5 YRS

Business licensed Certified factory

Manufactory Supplier of fine chemicals,pharmaceutical materials

3,5-Dichloroiodobenzene

CAS No.: 3032-81-3

Grade: industrial Grade

Content: 98%

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Guide of 1,3-Dichloro-5-iodobenzene

Description
Basic Attributes
Characteristics
Safety Information
Use and Manufacturing
Computed Properties
Recommended Suppliers
Latest News
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1,3-Dichloro-5-iodobenzene

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