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OXT 101

OXT 101 structure

CAS No:
3047-32-3
Formula:
C6H12O2
Chemical Name:
OXT 101
Synonyms:
3-Oxetanemethanol,3-ethyl-;3-Ethyl-3-oxetanemethanol;3-Ethyl-3-(hydroxymethyl)oxacyclobutane;3-Hydroxymethyl-3-ethyloxetane;3-Ethyl-3-(hydroxymethyl)oxetane;3-Ethyl-3-methyloloxetane;EOXA;Cyracure UVR 6000;Aron Oxetane OXT 101;OXA;OXA (oxetane);OXT 101;UVR 6000;Eternacoll EHO;(3-Ethyloxetan-3-yl)methanol;Aron Oxetane OXA;EHO;Trimethylolpropane oxetane;3-Ethyl-3-oxetanylmethyl alcohol;Syna OXA-S 101;S 101;Synasia S 101;TCM 101;3-Ethyl-3-hydroxymethyloxethane;Uvicure S 130;Doublemer 401;346425-95-4;473440-85-6
Categories:
Organic Chemistry > Coordination Complexes

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Description

clear colorless liquid

Liquid

OXT 101 Basic Attributes

Molecular Weight：

116.16

Exact Mass：

116.16

EC Number：

221-254-0

UNII：

622325VBYO

DSSTox ID：

DTXSID8062812

HScode：

2932999099

Characteristics

PSA：

29.5

XLogP3：

0.2

Appearance：

Liquid

Density：

1.0±0.1 g/cm3

Boiling Point：

84 °C @ Press: 2.8 Torr

Flash Point：

86.5±12.7 °C

Refractive Index：

1.443

Water Solubility：

Miscible in water.

Safety Information

Transport codes：

NONH for all modes of transport

wgk germany：

hazard class code：

R22;R36/37/38

safety instructions：

37/39-26

Marks：

Xn:Harmful;

Precautionary statement(s)：

P261, P264, P272, P273, P280, P302+P352, P305+P351+P338, P321, P333+P313, P337+P313, P363, P501

Hazard Statements：

H317

GHS Classification：

|Warning|H317 (55.28%): May cause an allergic skin reaction [Warning Sensitization, Skin]|P261, P264, P272, P273, P280, P302+P352, P305+P351+P338, P321, P333+P313, P337+P313, P363, and P501|Aggregated GHS information provided by 322 companies from 3 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.

OXT 101 Use and Manufacturing

Methods of Manufacturing

100g, diethyl carbonate 132g, potassium hydroxide 0.25g, bottle and ethanol 10 ml is added during the reaction. After heating at reflux for 2 hours, under atmospheric pressure, 150 °C by distillation in the greater part of the solvent is removed, a crude product is obtained. Furthermore, in a vacuum distillation is, for the purification of the crude product is obtained. 120 °C and 0.1torr compd. a1 (colorless liquid) is under a pressure, which is collected by the yield 64.7percent. Next, 82g compd. a1, pyridine 111g, and dichlomethane 400 ml bottles which are added to the reaction. The mixture is stirred under nitrogen, then cooled to 5° C -0 °C. 4-bromobenzoyl chloride in 200 ml of dichlomethane soln.of, 0 ° C-5 ° C during the reaction of the drop in the bottle. After completion of the addition, reaction bottle is warmed to room temperature, the stirring time is 8, the bottle 500 ml of water is added during the reaction, which is 5 min. The organic layer is collected, 100 ml of the water layer is extracted using dichlomethane 2 times. The organic layer is collected, in order to adjust the pH value to 7 in about 100 ml of the salt water. Next, an organic layer is collected, 20g is 30 minutes of drying with anhydrous sodium sulfate, then filtered. In order to obtain compd. a2, somas conc. under reduced pressure, the petroleum ether and ethyl acetate (9:1) [...] purified by using a flat, it is further chilled in ethanol recrystallization, 68.7percent yield. The purity of compd. a2 (gas chromatography (GC) analysis by a) is, at 98.109percent, and, the melting point (mp) compd. a2, 50.63 ° C-52.56 ° C.

Uses

Adhesives and sealant chemicals

Ink, toner, and colorant products

Production

100,000 - 500,000 lb

Manufacturing Info：

Adhesive manufacturing|3-Oxetanemethanol, 3-ethyl-: ACTIVE

Computed Properties

Molecular Weight:116.16
XLogP3:0.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:116.083729621
Monoisotopic Mass:116.083729621
Topological Polar Surface Area:29.5
Heavy Atom Count:8
Complexity:76.6
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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