p-Isopropenylphenol
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p-Isopropenylphenol
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CAS No:
4286-23-1
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Formula:
C9H10O
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Chemical Name:
p-Isopropenylphenol
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Synonyms:
Phenol,4-(1-methylethenyl)-;Phenol,p-isopropenyl-;4-(1-Methylethenyl)phenol;p-Isopropenylphenol;4-Isopropenylphenol;p-Hydroxy-α-methylstyrene;4-Hydroxy-α-methylstyrene;2-(4-Hydroxyphenyl)propene;4-(1-Propen-2-yl)phenol;α-Methyl-p-hydroxystyrene;4-(Methylethenyl)phenol
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CAS No:
p-Isopropenylphenol Use and Manufacturing
(2) Production of hydroquinone 84 g (0.201 mole) of the resulting p-isopropenyl phenol solution, 21.46 g (0.188 mole) of 30% aqueous hydrogen peroxide, and 10.0 g of an octanol solution containing 2.00 g of 98% sulfuric acid were maintained respectively at about 35 C., and simultaneously and continuously added dropwise to a flask and mixed. The reaction was an exothermic reaction. By cooling, the temperature of the inside of the flask was maintained at 35 C. After the addition, the mixture was stirred for 1 hour. Then, 25 g of sodium sulfite as a saturated aqueous solution was added to neutralize the sulfuric acid and decompose the unreacted peroxide. On standing, the reaction mixture separated into two layers. The aqueous layer was separated, and then, the organic layer was extracted four times with 150 ml of hot water each time. The water extracts containing acetone were combined, and concentrated, and cooled.
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