3,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-one
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3,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-one
structure -
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CAS No:
69225-59-8
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Formula:
C11H18O3
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Chemical Name:
3,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-one
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Synonyms:
1,5-Dioxaspiro[5.5]undecan-9-one,3,3-dimethyl-;3,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-one;1,4-Cyclohexanedione mono(2,2-dimethyltrimethylene ketal)
- Categories:
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CAS No:
3,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-one Basic Attributes
198.26
198.26
273-918-4
DTXSID10219262
2932999099
Characteristics
35.5
1
White to yellowish powder
1.1±0.1 g/cm3
48-49.5 °C @ Solvent: Hexane
70 °C @ Press: 0.05 Torr
123.3±13.8 °C
1.484
Safety Information
NONH for all modes of transport
3
R36/37/38
S24/25
P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, P501
H315
|Warning|H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]|P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, and P501|Aggregated GHS information provided by 2 companies from 2 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.
3,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-one Use and Manufacturing
6.1mg (0.02mmol) of sodiuim 2-iodobenzenesulfonate prepared by Preparation Example 4, 0.49g (0.8mmol) of powdered Oxone (registered trademark), 0.5g (3.5mol) of anhydrous sodium sulfate and 200mg (1mmol) of 3, 3-dimethyl-1, 5-dioxaspiro[5.5]undecan-9-ol were added to 5ml of ethyl acetate, and the mixture was heated at 70 °C while being stirred under a nitrogen for eight hours. 3, 3-Dimethyl-l, 5-dioxaspiro[5.5]undecan-9-one.; A continuous extraction apparatus is assembled. A 500 mL extraction solvent pot is charged with 250 mLπ-hexane and 5.00 g sodium bicarbonate. An oil bath is heated to 90°C. A 500 mL reaction pot is charged with 82.5 g (0.792 mol, 2.33 equiv) neopentyl glycol, 338 mLH
1,4-Cyclohexanedione mono(2,2-dimethyltrimethylene ketal)is a reagent used in the preparation of carbazole derivatives.
Computed Properties
Molecular Weight:198.26
XLogP3:1
Hydrogen Bond Acceptor Count:3
Exact Mass:198.125594432
Monoisotopic Mass:198.125594432
Topological Polar Surface Area:35.5
Heavy Atom Count:14
Complexity:223
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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