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6-AMINOISOQUINOLINE

6-AMINOISOQUINOLINE structure

CAS No:
23687-26-5
Formula:
C9H8N2
Chemical Name:
6-AMINOISOQUINOLINE
Synonyms:
6-AMINOISOQUINOLINE;6-aminoisoquanoline;6-Isoquinolinamine;Isoquinoline-6-amine;Isoquinolin-6-ylamine;Isoquinolin-6-amine, 6-Amino-2-azanaphthalene;Isoquinoline,6-amino- (7CI,8CI)
Categories:
Pharmaceutical Intermediates > Ophthalmic Agents

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6-AMINOISOQUINOLINE Basic Attributes

Molecular Weight：

144.17

Exact Mass：

144.068741

EC Number：

DSSTox ID：

DTXSID70343315

HScode：

2933499090

Characteristics

PSA：

38.9

XLogP3：

1.6

Density：

1.2±0.1 g/cm3

Melting Point：

211-212 °C(Solv: benzene (71-43-2))

Boiling Point：

343.1°C at 760 mmHg

Flash Point：

188.1±7.6 °C

Refractive Index：

1.708

Vapor Pressure：

7.2E-05mmHg at 25°C

Safety Information

hazard class code：

22-36

safety instructions：

Marks：

Precautionary statement(s)：

P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, P501

Hazard Statements：

H315

GHS Classification：

|Warning|H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]|P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, and P501|Aggregated GHS information provided by 2 companies from 2 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.

6-AMINOISOQUINOLINE Use and Manufacturing

A mixture of 1u (100 mg, 0.81 mmol), hydrazine hydrate (121.5mg, 2.43 mmol), and SS-Rh (370 mg, 2 molpercent Rh) were taken in an oven dried reaction tube equipped with screw cap. 0.5 ml of PEG-400 was added into the reaction mixture. The reaction was then irradiated in a microwave apparatus at 80°C , 80 W for 10 min with a pressure of 80 Psi. After cooling to ambient temperature in the microwave cavity the reaction mixture was extracted with ethyl acetate (3x2 ml) and water (1ml). The combined organic layer wasdried over anhydrous NaReference Example 1Step 3. Step 3. Example 41 - Synthesis of Compound 62; 1. 200 mg (1.35 mmol) of 1. 200 mg (1.35 mmol) of

Computed Properties

Molecular Weight:144.17
XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Exact Mass:144.068748264
Monoisotopic Mass:144.068748264
Topological Polar Surface Area:38.9
Heavy Atom Count:11
Complexity:136
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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