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9-[1,1'-Biphenyl-4-yl]-3-bromo-9H-carbazole

9-[1,1'-Biphenyl-4-yl]-3-bromo-9H-carbazole structure

CAS No:
894791-46-9
Formula:
C24H16BrN
Chemical Name:
9-[1,1'-Biphenyl-4-yl]-3-bromo-9H-carbazole
Synonyms:
9-Biphenyl-3-yl-3-broMo-9H-carbazole;3-bromo-9-(biphenyl-4-yl)-9H-carbazole;9-(4-Biphenylyl)-3-bromocarbazole;3-Bromo-9-(4-biphenylyl)carbazole;9-[1,1'-Biphenyl-4-yl]-3-bromo-9H-carbazole;9-(biphenyl-4-yl)-3-bromo-9H-carbazole;9H-Carbazole, 9-[1,1'-biphenyl]-4-yl-3-broMo-3-BroMo-9-(4-biphenylyl)carbazole;9-Biphenyl-4-yl-3-broMo-9H-carbazole(3BBPC)
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Pharmaceutical Intermediates > Oled Material Intermediate

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Description

White crystalline powder

9-[1,1'-Biphenyl-4-yl]-3-bromo-9H-carbazole Basic Attributes

Molecular Weight：

398.29

Exact Mass：

397.046600

DSSTox ID：

DTXSID20694804

HScode：

2933990090

Characteristics

PSA：

4.9

XLogP3：

7.3

Density：

1.32

Melting Point：

153.0 to 157.0 °C

Boiling Point：

552°C at 760 mmHg

Flash Point：

287.6±27.9 °C

Refractive Index：

1.670

Safety Information

Precautionary statement(s)：

P264, P280, P302+P352, P305+P351+P338, P321, P332+P313, P337+P313, P362

Hazard Statements：

H315

GHS Classification：

|Warning|H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]|P264, P280, P302+P352, P305+P351+P338, P321, P332+P313, P337+P313, and P362|The GHS information provided by 1 company from 1 notification to the ECHA C&L Inventory.

9-[1,1'-Biphenyl-4-yl]-3-bromo-9H-carbazole Use and Manufacturing

3.1 g (lOmmol) of 9-(4-biphenylyl)carbazole was dissolved in 100 mL of EPO Step 2: Synthesis of 9-(biphenyl-4-yl)-3-bromo-9H-carbazole][0588] A synthetic scheme of 9-(biphenyl-4-yl)-3-bromo-9H-carbazole in Step 2 is shown in the following (N-2).[0589] To a flask including 3-bromo-9H-carbazole and 4-iodo-1, 1′-biphenyl, 0.03 eq. of tris(dibenzilideneacetone)dipalladium(0) (PdB aniline (10mmol, 1 . 69g), 3, 6-dibromo-9-phenyl carbazole (11mmol, 4 . 41g) by adding 100 ml three-neck bottle, cuprous iodide is added under nitrogen (3mmol, 0 . 57g), potassium carbonate (30mmol, 4 . 15g), O-phenan throline (3mmol, 0 . 54g), 50mLN, N dimethyl formamide solution, 155 °C sleepovers reaction. After the reaction, water washing, extraction, drying of the organic layer, the solvent after evaporation to dryness, to obtain the product C-1 silica gel chromatography (2.44g, y = 50percent),

Computed Properties

Molecular Weight:398.3
XLogP3:7.3
Rotatable Bond Count:2
Exact Mass:397.04661
Monoisotopic Mass:397.04661
Topological Polar Surface Area:4.9
Heavy Atom Count:26
Complexity:465
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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Guide of 9-[1,1'-Biphenyl-4-yl]-3-bromo-9H-carbazole

Description
Basic Attributes
Characteristics
Safety Information
Use and Manufacturing
Computed Properties
Recommended Suppliers
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9-[1,1'-Biphenyl-4-yl]-3-bromo-9H-carbazole

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