Acetic acid, 2-hydrazinyl-, ethyl ester, hydrochloride (1:1)
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Acetic acid, 2-hydrazinyl-, ethyl ester, hydrochloride (1:1)
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CAS No:
6945-92-2
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Formula:
C4H10N2O2.ClH
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Chemical Name:
Acetic acid, 2-hydrazinyl-, ethyl ester, hydrochloride (1:1)
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Synonyms:
Acetic acid,2-hydrazinyl-,ethyl ester,hydrochloride (1:1);Acetic acid,hydrazino-,ethyl ester,monohydrochloride;Acetic acid,hydrazino-,ethyl ester,hydrochloride;Ethyl hydrazineacetate monohydrochloride;Hydrazineacetic acid ethyl ester hydrochloride;(Carbethoxymethyl)hydrazine hydrochloride;Ethyl hydrazinoacetate hydrochloride;Ethyl hydrazineacetate hydrochloride;Hydrazinoacetic acid ethyl ester hydrochloride;2-Hydrazinylacetic acid ethyl ester hydrochloride;Ethyl 2-(hydrazinyl)acetate hydrochloride;Ethyl hydrazinoacetate monohydrochloride;Ethyl 2-hydrazinoacetate hydrochloride
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CAS No:
Acetic acid, 2-hydrazinyl-, ethyl ester, hydrochloride (1:1) Basic Attributes
154.6
154.050903
230-104-3
2928000090
Safety Information
IRRITANT
NONH for all modes of transport
3
22-24/25
P261, P264, P270, P271, P280, P301+P312, P302+P352, P304+P340, P305+P351+P338, P312, P321, P330, P332+P313, P337+P313, P362, P403+P233, P405, P501
H302
Acetic acid, 2-hydrazinyl-, ethyl ester, hydrochloride (1:1) Use and Manufacturing
A solution of ethyl 2-hydrazinylacetate hydrochloride (1.0 g, 6.5 mmol) and DIEA (1.24 mL, 7.5 mmol) in toluene was stirred at room temperature. After 15 min, 4, 4-dimethyl-3-oxopentanenitrile (937 mg, 7.5 mmol) was added, and the reaction was stirred at reflux overnight. After cooling, water was added and the resulting mixture was extracted with EtOAc (x3). The combined organic layers were dried over MgSO4, filtered and concentrated under vacuum to give 1.5 g of 35 as a brown solid. This material was used without further purification.
Ethyl hydrazinoacetate hydrochloride has a wide range of applications in the laboratory research and development process and the chemical and pharmaceutical synthesis process.
Recommended Suppliers of Acetic acid, 2-hydrazinyl-, ethyl ester, hydrochloride (1:1)
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InquiryUnit Price: $100 /KG EXWCAS No.: 6945-92-2Grade: Pharmaceutical GradeContent: 99%
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