H-CHA-OME HCL
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H-CHA-OME HCL
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CAS No:
17193-39-4
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Formula:
C10H20ClNO2
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Chemical Name:
H-CHA-OME HCL
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Synonyms:
BETA-CYCLOHEXYL-L-ALANINE METHYL ESTER HYDROCHLORIDE;H-CHA-OME HCL;L-CYCLOHEXYLALANINE METHYL ESTER HCL;L-2-AMINO-3-CYCLOHEXYL-PROPIONIC ACID METHYL ESTER HYDROCHLORIDE;L-2-AMINO-3-HEXAHYDROPHENYLPROPIONIC ACID METHYL ESTER HYDROCHLORIDE;3-CYCLOHEXYL-L-ALANINE METHYL ESTER HYDROCHLORIDE;(S)-(-)-Cyclohexylalanine methyl ester hydrochloride;(S)-Methyl 2-aMino-3-cyclohexylpropanoate hydrochloride
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CAS No:
H-CHA-OME HCL Use and Manufacturing
General procedure: For the synthesis of compounds 2a, 2c–2g, we used slightly modificated known procedure [1]. To a stirred solution of amino acid (32.2mmol) in dry methanol (100mL) was added drop-wise thionyl chloride (64.4mmol). The temperature was kept between−10 and−5°C. After complete addition, the reaction was stirred at RT overnight. After 16h, the solution was evaporated to dryness. The product was diluted with EtOAc and collected by filtration. The residue was dried under reduced pressure to give an amino acid methyl ester hydrochloride as white crystalline powder. The yields were higher in all experiments than 80percent. Melting point and
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