β-Cyclohexyl-L-alanine methyl ester hydrochloride
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β-Cyclohexyl-L-alanine methyl ester hydrochloride
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CAS No:
17193-39-4
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Formula:
C10H19NO2.ClH
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Chemical Name:
β-Cyclohexyl-L-alanine methyl ester hydrochloride
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Synonyms:
BETA-CYCLOHEXYL-L-ALANINE METHYL ESTER HYDROCHLORIDE;H-CHA-OME HCL;L-CYCLOHEXYLALANINE METHYL ESTER HCL;L-2-AMINO-3-CYCLOHEXYL-PROPIONIC ACID METHYL ESTER HYDROCHLORIDE;L-2-AMINO-3-HEXAHYDROPHENYLPROPIONIC ACID METHYL ESTER HYDROCHLORIDE;methyl (2S)-2-amino-3-cyclohexylpropanoate hydrochloride;L-CYCLOHEXYLALANINEMETHYLESTERHYDROCHLOERIDE;(S)-Methyl 2-aMino-3-cyclohexylpropanoate hydrochloride
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CAS No:
β-Cyclohexyl-L-alanine methyl ester hydrochloride Basic Attributes
221.72
221.11800
White to off-white
29224999
β-Cyclohexyl-L-alanine methyl ester hydrochloride Use and Manufacturing
General procedure: For the synthesis of compounds 2a, 2c–2g, we used slightly modificated known procedure [1]. To a stirred solution of amino acid (32.2mmol) in dry methanol (100mL) was added drop-wise thionyl chloride (64.4mmol). The temperature was kept between−10 and−5°C. After complete addition, the reaction was stirred at RT overnight. After 16h, the solution was evaporated to dryness. The product was diluted with EtOAc and collected by filtration. The residue was dried under reduced pressure to give an amino acid methyl ester hydrochloride as white crystalline powder. The yields were higher in all experiments than 80percent. Melting point and
H-beta-Cyclohexyl-Ala-OMe·HCl is used in the preparation of novel fluoropeptidomimetics, which are potential protease inhibitors.
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β-Cyclohexyl-L-alanine methyl ester hydrochloride
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