2-AMINO-5-CHLOROBENZYL ALCOHOL
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2-AMINO-5-CHLOROBENZYL ALCOHOL
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CAS No:
37585-25-4
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Formula:
C7H8ClNO
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Chemical Name:
2-AMINO-5-CHLOROBENZYL ALCOHOL
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Synonyms:
RARECHEM AL BD 1516;(2-AMINO-5-CHLOROPHENYL)METHANOL;2-AMINO-5-CHLOROBENZYL ALCOHOL;2-Amino-5-chlorobenzenemethanol
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CAS No:
Safety Information
3
36/37/38
26-37/39
Xi
P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, P501
H315
|Warning|H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]|P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, and P501|Aggregated GHS information provided by 42 companies from 2 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.
2-AMINO-5-CHLOROBENZYL ALCOHOL Use and Manufacturing
General procedure: To a suspension of lithium aluminum hydride (20.4 mmol) in THF (10 mL) was added benzoic acid (8.5 mmol) dissolved in THF (24 mL) dropwise over 20 minutes at room temperature. The reaction continued to stir at room temperature for 3.5 h, and then was quenched at 0 °C with HPreparation of (2-amino-phenyl)-methanols (2) by reduction of 2-amino- benzoic acids (3) - General procedure; [0078] 2-Amino-benzoic acid (14 mmol) in dry diethyl ether (15 ml_) is added dropwise to an ice cooled solution of lithium aluminum hydride (15 mmol) in dry diethyl ether (100 mL) and stirred at room temperature for 2 h. Water (8 ml) is added dropwise, followed by 1M aqueous sodium hydroxide solution (13 mL). The organic layer is collected, dried over sodium sulfate and concentrated under reduced pressure. The crude product is used in the next step without further purification.; (2-Amino-5-chloro-phenyl)-methanol; Yield 88percent;
Computed Properties
Molecular Weight:157.60
XLogP3:1.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:157.0294416
Monoisotopic Mass:157.0294416
Topological Polar Surface Area:46.2
Heavy Atom Count:10
Complexity:110
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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