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9,10-Diaminophenanthrene

9,10-Diaminophenanthrene structure

CAS No:
53348-04-2
Formula:
C14H12N2
Chemical Name:
9,10-Diaminophenanthrene
Synonyms:
9,10-Phenanthrenediamine;9,10-Diaminophenanthrene;NSC 80191
Categories:
Chemical Reagents > Organic Reagents

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9,10-Diaminophenanthrene Basic Attributes

Molecular Weight：

208.26

Exact Mass：

208.26

EC Number：

258-490-9

NSC Number：

80191

DSSTox ID：

DTXSID30201508

HScode：

2921590090

Characteristics

PSA：

XLogP3：

3.1

Density：

1.283g/cm3

Melting Point：

160 °C @ Solvent: Benzene

Boiling Point：

457.6°C at 760 mmHg

Flash Point：

276.6ºC

Refractive Index：

1.816

Storage Conditions：

2-8°C

Safety Information

Transport codes：

NONH for all modes of transport

wgk germany：

hazard class code：

36/37/38

safety instructions：

26-37/39

Marks：

Precautionary statement(s)：

P261-P305 + P351 + P338

Hazard Statements：

H315-H319-H335

GHS Classification：

|Warning|H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]|P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, and P501|Aggregated GHS information provided by 38 companies from 1 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.

9,10-Diaminophenanthrene Use and Manufacturing

Add 1-3, 200 mmol in the reaction vessel; 300 mmol of ammonia water, 600 mmol of potassium t-butoxide, 32 mol of Pd2 (dba), ultrasonically deoxidized toluene, stir and dissolve, replace the air three times, and add the ligand tri-tert-butylphosphorus. 4percent, 8 mmol, the air was replaced again three times, and the reaction was refluxed for 6 h. Cool to room temperature, add enough dichloromethane to completely dissolve the product, and pass a small amount of silica gel funnel to remove the catalyst and salt. The filtrate was concentrated to a viscous condition and subjected to column chromatography to afford product 62-2, 170 mmol.General procedure: Aniline (1.0 mmol), aldehyde (1.0 mmol) and ammonium acetate (7.0 mmol) was added into glacial acetic acid (2 mL) at room temperature for 2, 4 and 6 where as aldehyde (1.0mmol) and ammonium acetate (7.0 mmol) was added into glacial acetic acid (2 mL) for 1, 3, 5 and 7. The resulting mixture was stirred for 4 h at 95 C. The completion of the reaction was monitored by thin layer chromatography. After cooling, the reaction mixture was dumped into cold water. The resulting precipitate was filtered, washed with water and dried under vacuum. The white solid was purified with column chromatography.

Computed Properties

Molecular Weight:208.26
XLogP3:3.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Exact Mass:208.100048391
Monoisotopic Mass:208.100048391
Topological Polar Surface Area:52
Heavy Atom Count:16
Complexity:227
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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9,10-DIAMINOPHENANTHRENE

CAS No.: 53348-04-2

Grade: Industrial Grade

Content: 98%

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