Cyclohexyltrimethoxysilane
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Cyclohexyltrimethoxysilane
structure -
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CAS No:
17865-54-2
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Formula:
C9H20O3Si
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Chemical Name:
Cyclohexyltrimethoxysilane
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Synonyms:
Cyclohexane,(trimethoxysilyl)-;Silane,cyclohexyltrimethoxy-;(Trimethoxysilyl)cyclohexane;Cyclohexyltrimethoxysilane;C 2280
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CAS No:
Safety Information
36/37/38
26-36/37/39
P260, P264, P280, P301+P330+P331, P303+P361+P353, P304+P340, P305+P351+P338, P310, P321, P363, P405, P501
H314
|Danger|H226 (20.55%): Flammable liquid and vapor [Warning Flammable liquids]|P210, P233, P240, P241, P242, P243, P260, P261, P264, P271, P273, P280, P301+P330+P331, P302+P352, P303+P361+P353, P304+P340, P305+P351+P338, P310, P312, P321, P332+P313, P337+P313, P362, P363, P370+P378, P403+P233, P403+P235, P405, and P501|Aggregated GHS information provided by 77 companies from 5 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.
Cyclohexyltrimethoxysilane Use and Manufacturing
Hydrosilane (amount shown in Table 3) listed in Table 3 was added to a cyclohexene solution (0.5 mL) of Rh (Phebox-iPr) (OAc) 2 OH 2 (5.4 mg, 0.010 mmol) represented by the following formula added. After stirring at 50 ° C. for 12 hours, Pentadecane (42.5 mg, 55.2 muL, 0.20 mmol) was added and the yield of each product was determined by measuring GC. As a result, the product of Example 7 (n = 1) was obtained in a yield of 59percentThe product of Example 8 (n = 0) was obtained in 73percent yield.Lmol of 1-chloro bicyclo [1, 1, 1] pentane and 1. lmol of magnesium powder and 500 ml of dry tetrahydrofuran were mixed, Heated to reflux for 2h, cooled to room temperature, lh in the lmol Under N2 protection conditions, To the reaction flask was successively added 3. 6 g of N-methylpiperazine, 40ml is burning, stirring;At a temperature of 5 ° C, A solution of 16. 8 ml (2. 87 M) butyllithium-n-hexane was added dropwise, Dropping time is 20min;After the addition was completed at 5 ° C for 40 min, the reaction solution was added dropwise to the reaction solution. 9. 4 g of In N2 Under protection, three-necked flask with stirring and the funnel was added dropwise and THF150ml 100mmol isopropyl piperazine, in an ice bath, was slowly added dropwise through a dropping funnel 100mmol butyllithium dropwise after l to room temperature, the reaction after 1h.Under a 71/92 then cooled to 0°C 100mmol
Computed Properties
Molecular Weight:204.34
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:204.11817103
Monoisotopic Mass:204.11817103
Topological Polar Surface Area:27.7
Heavy Atom Count:13
Complexity:134
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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