4-BENZYLOXY-2-CHLOROPYRIMIDINE
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4-BENZYLOXY-2-CHLOROPYRIMIDINE
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CAS No:
108381-28-8
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Formula:
C11H9ClN2O
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Chemical Name:
4-BENZYLOXY-2-CHLOROPYRIMIDINE
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Synonyms:
4-BENZYLOXY-2-CHLOROPYRIMIDINE;PyriMidine, 2-chloro-4-(phenylMethoxy)-
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CAS No:
Characteristics
35
3
1.278±0.06 g/cm3(Predicted)
387.0±17.0 °C(Predicted)
187.9ºC
1.593
7.57E-06mmHg at 25°C
4-BENZYLOXY-2-CHLOROPYRIMIDINE Use and Manufacturing
Step 1. A mixture formed by 2.26 g (20.1 mmol, 1 equiv.) of potass tert-butoxide and 4.3 g (40.2 mmol, 2 equiv.) of compound phenylmethanol in 10 ml of THF was heated under reflux temperature for half an hour. The reaction mixture was cooled down to 0 To a cooled (1-2° C.) suspension of sodium hydride (60percent in mineral oil) (1.5 equiv) in 250 ml THF, benzyl alcohol (1.0 equiv.) was added dropwise and the mixture stirred 30 min under N
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