2-AMino-3-forMyl-4-chloropyridine
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2-AMino-3-forMyl-4-chloropyridine
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CAS No:
884004-48-2
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Formula:
C6H5ClN2O
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Chemical Name:
2-AMino-3-forMyl-4-chloropyridine
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Synonyms:
2-Amino-4-chloronicotinaldehyde;2-AMINO-3-FORMYL-4-CHLOROPYRIDINE;2-Amino-4-chloropyridine-3-carbaldehyde;2-AMINO-4-CHLORO-PYRIDINE-3-CARBALDEHYDE;3-Pyridinecarboxaldehyde, 2-amino-4-chloro-;SCHEMBL1863142;DTXSID80673079;BCP31178;KS-00000PN8;1504AJ
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CAS No:
Safety Information
|Warning|H302 (100%): Harmful if swallowed [Warning Acute toxicity, oral]|P261, P264, P270, P271, P280, P301+P312, P302+P352, P304+P312, P304+P340, P305+P351+P338, P312, P321, P322, P330, P332+P313, P337+P313, P362, P363, P403+P233, P405, and P501|The GHS information provided by 1 company from 1 notification to the ECHA C&L Inventory.
2-AMino-3-forMyl-4-chloropyridine Use and Manufacturing
In a round-bottom flask, equipped with a stirrer, thermometer and reflux condenser, mix in the specified order: 135 mL of dry tetrahydrofuran (THF), 20 g (0.169 mol) of N, N, N′, N′-tetramethylethylenediamine, and 15.7 g (0.068 mol) of BCD-BTK-4-11. Cool the resulting mixture to -78 °; add, dropwise, 68 mL of 2.5M n-butyllithium in hexane, maintaining the temperature. After that, allow the reaction mass to stand for another 30 minutes. Add 15 g (0.2 mol) of DMF, maintaining the temperature at -78 °. After 1 hour, stop the cooling and allow the reaction mixture to warm to room temperature. Allow to stand for another hour. Add, while cooling, 30 mL of methanol and 150 mL of NH
Computed Properties
Molecular Weight:156.57
XLogP3:1.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:156.0090405
Monoisotopic Mass:156.0090405
Topological Polar Surface Area:56
Heavy Atom Count:10
Complexity:131
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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2-AMino-3-forMyl-4-chloropyridine
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