5-BroMo-1,2,3-triazine

One step up the crude was added methylene chloride (200 mL) and water (76 mL), cooled to 0 , sodium periodate (29.4g, 137mmol) with stirring. After the addition was complete the reaction was stirred for 12 hours 0 . Warmed to 25 , liquid separation, the aqueous phase was extracted with dichloromethane (100mL × 3), the organic phases were combined, saturated brine (250mL), dried over anhydrous sodium sulfate, filtered, and the filtrate was concentrated and the crude product was purified by silica gel column chromatography (petroleum ether: ethyl acetate = 10: 1) gave the title compound as a white solid (8.8g, yield 73.5percent in two steps).To a solution of compound S2 (1 g, crude) in DCM (15 mL) and water (5 mL) was added NaIO

Molecular Weight:159.97
Hydrogen Bond Acceptor Count:3
Exact Mass:158.94321
Monoisotopic Mass:158.94321
Topological Polar Surface Area:38.7
Heavy Atom Count:7
Complexity:52.1
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes