3-broMo-4H,5H-thieno[3,2-c]pyridin-4-one
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3-broMo-4H,5H-thieno[3,2-c]pyridin-4-one
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CAS No:
799293-83-7
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Formula:
C7H4BrNOS
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Chemical Name:
3-broMo-4H,5H-thieno[3,2-c]pyridin-4-one
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Synonyms:
3-broMo-4H,5H-thieno[3,2-c]pyridin-4-one;3-BroMothieno[3,2-c]pyridin-4(5H)-one;3-broMo-4-hydroxy-[3,2-c]-thienopyridine;3-BROMO-4-HYDROXYTHIENO[3,2-C]PYRIDINE;3-Bromothieno[3,2-c]pyridin-4-ol;3-Bromothieno[3,2-c]pyridin-4(5H)
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CAS No:
3-broMo-4H,5H-thieno[3,2-c]pyridin-4-one Basic Attributes
230.08176
228.92000
DTXSID10593953
2934999090
Safety Information
UN 3260 8 / PGIII
3
25-34-36
26-36/37/39-45
T,C
P280-P305 + P351 + P338-P310
H314
3-broMo-4H,5H-thieno[3,2-c]pyridin-4-one Use and Manufacturing
202.3 Diphenyl ether (40 ml) was heated to boiling (bp. 259° C.) and treated cautiously with a crude solution of (E)-3-(4-bromo-thiophen-2-yl)-acryloyl azide. The volatiles were distilled off during the slow addition and the reaction heated for an additional 1 h. The reaction was then allowed to cool to room temperature and diluted with petroleum spirit 40-60° C. (100 ml) to afford a precipitate which was filtered, washed with hot petroleum spirit 40-60° C. (20 ml), and air and oven dried to yield a yellow solid (1.16 g, 39percent).
3-broMo-4H,5H-thieno[3,2-c]pyridin-4-one
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