2-Bromo-3-trifluoromethylpyridine
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2-Bromo-3-trifluoromethylpyridine
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CAS No:
175205-82-0
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Formula:
C6H3BrF3N
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Chemical Name:
2-Bromo-3-trifluoromethylpyridine
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Synonyms:
2-Bromo-3-trifluoromethylpyridine 2-Bromo-3-(trifluoromethyl)pyridine;BUTTPARK 27\06-85;PYRIDINE, 2-BROMO-3-(TRIFLUOROMETHYL)-;2-Bromo-3-(trifluoromethyl)pyridine 98%;2-Bromo-3-(trifluoromethyl)pyridine98%;16189 2-BROMO-3-TRIFLUOROMETHYLPYRIDINE;16189;Bromotrifluoromethylpyridine 23()---
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CAS No:
Characteristics
12.9
2.8
Light yellow Cryst
1.707±0.06 g/cm3(Predicted)
37-41 °C
76°C8mm
84 °F
1.471
0.000858mmHg at 25°C
Safety Information
II
4.1
UN 2926 4.1/PG 3
3
11-25-37/38-41-36/37/38
26-36/37/39-45
F,T,Xi
Irritant
P210-P261-P264-P280-P301 + P310-P305 + P351 + P338
H228-H300-H315-H318-H335
2-Bromo-3-trifluoromethylpyridine Use and Manufacturing
Weigh 4.2g of Diosgenin, 0.8 g of sodium ethoxide was dissolved in 100 mL of n-propanol in a 500 mL three-necked flask, and then 2.5 g of 3-trifluoromethyl-2-bromo-pyridine was added, and the mixture was heated with stirring at 60 C for 36 hours. TLC (developing solvent: petroleum Ether-ethyl acetate (1: 1), developer: 5% phosphomolybdic acid ethanol solution) Detect all reactions of diosgenin, evaporate n-propanol, cool to room temperature, add 80 mL of water, and extract 3 times with chloroform (100 mL × 3), TLC followed the process of separation and purification of the product, the extract was recovered chloroform, and the solid was dried at 60 C. for 4 h to obtain 3.0 g of the product as a light yellow powder.
Recommended Suppliers of 2-Bromo-3-trifluoromethylpyridine
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2-Bromo-3-trifluoromethylpyridine
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