3-BROMO-5-(TRIFLUOROMETHYL)TOLUENE

(0510) (0511) 15 In a 50 ml_ two-necked flask equipped with a reflux condenser, magnesium turnings (391 mg, 16.1 mmol) were combined with THF (7 ml). 1 -Bromo-3-methyl-5-(trifluoromethyl)benzene (3.85 g, 2.5 ml, 16.1 mmol) dissolved in THF (12.2 ml) was added drop wise during which the reaction initiated and warming up to 50C. During the addition of the remaining solution the temperature was kept at kept at 38C. The mixture was heated to 38C for 1 h, then allowed to 0 cool down to room temperature. This solution was used as such1-ethenyl-3-methyl-5-(trifluoromethyl)benzene To EXAMPLE 8 A mixture of 30 ml of hydrogen fluoride and 50 g of 2-methyl-5-bromobenzotrifluoride is heated at 140 C. under a pressure of nitrogen of 28 bar for 5 hours. After cooling down, the organic phase was analyzed. 7.2% by weight of

Molecular Weight:239.03
XLogP3:3.9
Hydrogen Bond Acceptor Count:3
Exact Mass:237.96050
Monoisotopic Mass:237.96050
Heavy Atom Count:12
Complexity:155
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes