2-Bromo-1-bromomethyl-5-chlorobenzene
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2-Bromo-1-bromomethyl-5-chlorobenzene
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CAS No:
66192-24-3
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Formula:
C7H5Br2Cl
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Chemical Name:
2-Bromo-1-bromomethyl-5-chlorobenzene
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Synonyms:
1-bromo-2-(bromomethyl)-4-chlorobenzene;2-Bromo-5-chlorobenzyl bromide;2-Bromo-1-bromomethyl-5-chlorobenzene;1-bromo-2-(bromomethyl)-4-chloro-benzene;ACMC-209ntz;SCHEMBL532613;2-Bromo-5-chlorobenzylBromide;CTK1J5106;DTXSID30474371;ANW-35157
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CAS No:
Safety Information
P260, P264, P280, P301+P330+P331, P303+P361+P353, P304+P340, P305+P351+P338, P310, P321, P363, P405, P501
H314
2-Bromo-1-bromomethyl-5-chlorobenzene Use and Manufacturing
20.5 g (100 mmol) of 2-bromo-5-chlorotoluene was dissolved in 200 ml of carbon tetrachloride, 0.2 g (1 mmol) of AIBN and 19.6 g (110 mmol) of N-bromosuccinimide were added thereto, the resulting mixture was refluxed for 2 hours and cooled to room temperature. The reaction mixture was washed with 50 ml of water twice and with 50 ml of a brine solution, dried over anhydrous MgS04, and distilled under a reduced pressure to obtain an oil containing a small amount of the starting material. The oil was dissolved in 20 ml of hexane, and recrystallized at room temperature to obtain ' 22.7 g (yield 80percent) of 2-bromo-l-bromomethyl-5-chlorobenzene. Step 1: l-bromo-2-(bromomethyl)-4-chlorobenzene; l-bromo-2-(bromomethyl)-4-chlorobenzene was prepared according to literature precedent (J. Am. Chem. Soc. 2002, 124 (7), 1354): a suspension of l-bromo-2-methyl-4-chlorobenzene (1 eq), NBS (1 eq) and benzoyl peroxide (0.004 eq) in CCl
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Business licensedTrader Supplier of pharmaceutical intermediates,excipients,plant extracts,food additives,CDMO,fine cheimcals,Octadecanedioic acid,Eicosanedioic AcidInquiryCAS No.: 66192-24-3Grade: Pharmaceutical GradeContent: 95%
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2-Bromo-1-bromomethyl-5-chlorobenzene
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