2-Bromo-3-hydroxybenzaldehyde
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2-Bromo-3-hydroxybenzaldehyde
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CAS No:
196081-71-7
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Formula:
C7H5BrO2
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Chemical Name:
2-Bromo-3-hydroxybenzaldehyde
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Synonyms:
2-BROMO-3-HYDROXYBENZOIC ACID;B90006;2-Bromo-3-formylphenol;Benzaldehyde, 2-broMo-3-hydroxy-;2-BroMo-3-hydroxybenzaldehyde, 95+%
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CAS No:
Safety Information
Xi
P261, P264, P270, P271, P273, P280, P301+P312, P302+P352, P304+P312, P304+P340, P305+P351+P338, P312, P321, P322, P330, P332+P313, P337+P313, P362, P363, P391, P403+P233, P405, P501
H302
|Warning|H302 (100%): Harmful if swallowed [Warning Acute toxicity, oral]|P261, P264, P270, P271, P273, P280, P301+P312, P302+P352, P304+P312, P304+P340, P305+P351+P338, P312, P321, P322, P330, P332+P313, P337+P313, P362, P363, P391, P403+P233, P405, and P501|Aggregated GHS information provided by 2 companies from 2 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.
2-Bromo-3-hydroxybenzaldehyde Use and Manufacturing
The suspension of 3-hydroxybenzaldehyde (5 g, 0.04 mol), iron powder (172 mg, 3 mmol) and sodium acetate (6.72 g, 0.08 mol) in acetic acid (40 mL) was warmed until a clear solution was obtained and then cooled to room temperature. To this mixture was dropwise added a solution of bromine in glacial acetic acid (10 mL) over 15 min. After the addition, the reaction mixture was stirred for 2 h and then poured into ice-water. The resulting mixture was extracted with dichloromethane (3x50 mL). The combined extracts were dried over anhydrous NaA suspension of 3-hydroxybenzaldehyde (5 g, 40 mmol), iron powder (172 mg, 3 mmol) and sodium acetate (6.72 g, 80 mmol) in acetic acid (40 mL) was warmed until a clear solution was obtained and then cooled to room temperature. To this mixture was added dropwise a solution of bromine (7.2 g, 45 mmol) in glacial acetic acid (10 mL) over 15 min. After the addition, the reaction mixture was stirred for 2 h and then poured into ice- water. The resulting mixture was extracted with dichloromethane (3x50 mL). The combined extracts were dried over anhydrous Na
A reactant used in the preparation of a class of benzoxaboroles antimalarial agents.
Computed Properties
Molecular Weight:201.02
XLogP3:1.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:199.94729
Monoisotopic Mass:199.94729
Topological Polar Surface Area:37.3
Heavy Atom Count:10
Complexity:127
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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