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9,10-Di(1-naphthyl)anthracene

9,10-Di(1-naphthyl)anthracene structure

CAS No:
26979-27-1
Formula:
C34H22
Chemical Name:
9,10-Di(1-naphthyl)anthracene
Synonyms:
9,10-DI-(1-NAPHTHYL)ANTHRACENE;9,10-DI-NAPHTHALEN-1-YL-ANTHRACENE;9,10-Di-(1-naphthyl);9,10-Di(-α-naphthyl)anthracen;9,10-Di(1-naphthayl)anthracene (purified by sublimation)
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Pharmaceutical Intermediates > Bulk Drug Intermediates

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9,10-Di(1-naphthyl)anthracene Basic Attributes

Molecular Weight：

430.54

Exact Mass：

430.172150

EC Number：

1312995-182-4

NSC Number：

90485

DSSTox ID：

DTXSID50293541

HScode：

2902909090

Characteristics

PSA：

XLogP3：

10.2

Density：

1.2±0.1 g/cm3

Melting Point：

360°C(lit.)

Boiling Point：

577.5°C at 760 mmHg

Flash Point：

304.1±22.8 °C

Refractive Index：

1.761

9,10-Di(1-naphthyl)anthracene Use and Manufacturing

General procedure: A 10-mL test tube equipped with a magnetic stirring bar and a cap was charged with9, 10-diphenyl-9, 10-epoxyanthracene (3a) (102 mg, 295 mumol), wet dichloromethane (600muL), triethylsilane (71.9 muL, 450 mumol), and trifluoroacetic acid (26.7 muL, 360 mumol). Themixture was stirred for 30 min, after which time TLC (hexanes-ethyl acetate = 3:1) indicatedcomplete consumption of 9, 10-diphenyl-9, 10-epoxyanthracene (3a). The reaction wasquenched with H2O and the aqueous layer was extracted with dichloromethane three times.The combined organic extracts were successively washed with saturated aqueous NaHCO3and brine, dried over anhydrous Na2SO4, and filtered. The organic solvents were removedunder reduced pressure to give a crude anthracene, which was purified by flash silica gelcolumn chromatography (hexanes-dichloromethane = 4:1) to afford 4a (91.4 mg, 277 mumol, 94%) as a pale yellow solid. Rf = 0.73 (hexanes-ethyl acetate = 3:1). The spectrum data of 4awere in complete agreement with those reported in the literature.5

Computed Properties

Molecular Weight:430.5
XLogP3:10.2
Rotatable Bond Count:2
Exact Mass:430.172150702
Monoisotopic Mass:430.172150702
Heavy Atom Count:34
Complexity:598
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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9,10-Di(1-naphthyl)anthracene

CAS No.: 26979-27-1

Content: 99.00%

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Guide of 9,10-Di(1-naphthyl)anthracene

Basic Attributes
Characteristics
Use and Manufacturing
Computed Properties
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9,10-Di(1-naphthyl)anthracene

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