ethylalpha-bromodiethylacetate
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ethylalpha-bromodiethylacetate
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CAS No:
6937-28-6
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Formula:
C8H15BrO2
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Chemical Name:
ethylalpha-bromodiethylacetate
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Synonyms:
2-BroMo-2-ethylbutyric Acid Ethyl Ester;Ethyl 2-BroMo-2-ethylbutyrate;NSC 41719;α-BroModiethylacetic Acid Ethyl Ester
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CAS No:
ethylalpha-bromodiethylacetate Use and Manufacturing
Add 0.1 mmol of primary amine compound, 0.2 mmol of ethyl 2-bromodimethylpropionate, 0.1 mmol of dimethyl butynedioate, and 0.2 mol of potassium acetate, and add 0.5 mL of methyl tert-butyl ether. In a reactor at 120 C, after reacting for 24 hours, cool to room temperature, then filter the solid impurities through diatomaceous earth, wash with dichloromethane 3 times to obtain the filtrate, then concentrate the filtrate, and then go through column chromatography or Purification by layer chromatography gave 14.9 mg of the target product in a yield of 45%.
An α-bromo tertiary ester used as a reagent in in organic synthesis.
Computed Properties
Molecular Weight:223.11
XLogP3:2.9
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:222.02554
Monoisotopic Mass:222.02554
Topological Polar Surface Area:26.3
Heavy Atom Count:11
Complexity:130
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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