 Home > Encyclopedia > N-DECYLBORONIC ACID

N-DECYLBORONIC ACID

N-DECYLBORONIC ACID structure

CAS No:
24464-63-9
Formula:
C10H23BO2
Chemical Name:
N-DECYLBORONIC ACID
Synonyms:
1-Decylboronic acid, 98%;Decylboronic acid;1-Decaneboronicacid (6CI);RARECHEM AH PB 0104;N-DECYLBORONIC ACID;Decylboronic acid, 98.8%
Categories:
Chemical Reagents > Organic Reagents

Request for Quotation

N-DECYLBORONIC ACID Basic Attributes

Molecular Weight：

186.1

Exact Mass：

186.179108

BRN：

1743934

DSSTox ID：

DTXSID70400492

HScode：

2931900090

Characteristics

PSA：

40.5

Density：

0.9±0.1 g/cm3

Melting Point：

76-78°C

Boiling Point：

297.1°C at 760 mmHg

Flash Point：

133.5±22.6 °C

Refractive Index：

1.434

Safety Information

hazard class code：

36/37/38

safety instructions：

26-36

N-DECYLBORONIC ACID Use and Manufacturing

Methods of Manufacturing

A 100mL flask was charged with 2.1M HBBr2Me2S in CH2Cl2(26.2 mL, ca. 55.0 mmol) and 1-decene (9.5 mL, 50.0 mmol) wasadded dropwise to the stirred solution at 20 °C. One molar BBr3 inCH2Cl2 (2.5 mL, 2.5 mmol) was added dropwise while the reactionmixture was cooled to 0 °C; the reaction was stirred for 15 min;then warmed spontaneously to 20 °C; and stirred for 30 min. Thesolution of boraneswas hydrolyzed by dropwise transfer to another flask containing a stirred mixture of Et2O (100 mL) and H2O (20 mL)at 0 °C then stirred for 20 min. The solution was transferred to aseparatory funnel with minimal exposure to air; the aqueous layerwas separated and discarded; the organic phase was washed withH2O (2 30 mL) and brine (2 30 mL); dried over MgSO4 andfiltered; then concentrated on a rotary evaporator. The yield of freeflowingwhite powder was 8.71 g, 93percent. 1H NMR δ 6.50 (s, 2H), 1.41(p, J 7.8, 7.2 Hz, 2H), 1.28 (s, 14H), 0.92-0.84 (m, 3H), 0.71 (t, J 7.8 Hz, 2H). 13C NMR δ 32.55, 32.07, 29.79, 29.73, 29.62, 29.50, 24.53, 23.50, 22.85, 14.28. 11B NMR d 32.32.

Uses

suzuki reaction

Computed Properties

Molecular Weight:186.10
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:9
Exact Mass:186.1791101
Monoisotopic Mass:186.1791101
Topological Polar Surface Area:40.5
Heavy Atom Count:13
Complexity:96.9
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

Recommended Suppliers of N-DECYLBORONIC ACID

HANGZHOU LEAP CHEM CO., LTD. Contact Supplier

CN
5 YRS

Business licensed

Trader Supplier of Intermediates,Building blocks,API,Silicones,Peptides,Lab chemicals,Biochemicals,Pharmaceuticals,Screening Compounds,Food Additives

n-Decylboronic acid

CAS No.: 24464-63-9

Content: 99.00%

Inquiry
Hangzhou Zentra Bio-Chemical Co., Ltd. Contact Supplier

CN
1 YR

Business licensed

Trader Supplier of pharmaceutical intermediates,excipients,plant extracts,food additives,CDMO,fine cheimcals,Octadecanedioic acid,Eicosanedioic Acid

Decylboronic Acid 24464-63-9

CAS No.: 24464-63-9

Grade: Pharmaceutical Grade

Content: 99%

Inquiry