oxacyclooctadecan-2-one
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oxacyclooctadecan-2-one
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CAS No:
5637-97-8
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Formula:
C17H32O2
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Chemical Name:
oxacyclooctadecan-2-one
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Synonyms:
17-Heptadecanolid;Oxacyclooctadecan-2-on;Oxacyclooctadecan-2-one;Oxacyclooctadecan;
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CAS No:
Analysis Methods
| Name | Column Shape | Active Phase(℃) | Retention index | Temperature Control | Method | Comments | Reference |
|---|---|---|---|---|---|---|---|
| Kovats' RI, non-polar column, temperature ramp | Capillary | HP-5 | 2028. | temperature ramp | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 260. C | Lopes, D.Strobl, H.Kolodziejczyk, P.14-Methylpentadecano-15-lactone (Muscolide): a new macrocyclic lactone from the oil of Angelica archangelica L.Chemistry and Biodiversity2004, 1, 12, 1880-1887. | |
| Kovats' RI, non-polar column, temperature ramp | Capillary | DB-Wax | 2433. | temperature ramp | 30. m/0.32 mm/0.25 μm, He, 40. C @ 5. min, 3. K/min; Tend: 220. C | Lopes, D.Strobl, H.Kolodziejczyk, P.14-Methylpentadecano-15-lactone (Muscolide): a new macrocyclic lactone from the oil of Angelica archangelica L.Chemistry and Biodiversity2004, 1, 12, 1880-1887. | |
| Kovats' RI, non-polar column, temperature ramp | Capillary | HP-5MS | 2042.3 | custom temperature program | 30. m/0.25 mm/0.25 μm, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min) | Andriamaharavo, N.R.Retention Data. NIST Mass Spectrometry Data Center.NIST Mass Spectrometry Data Center, 2014. | |
| Kovats' RI, non-polar column, temperature ramp | Capillary | SPB-5 | 2051. | temperature ramp | 50. m/0.32 mm/0.25 μm, He, 3. K/min, 240. C @ 20. min; Tstart: 60. C | Doneanu, C.Anitescu, G.Supercritical carbon dioxide extraction of Angelica archangelica L. root oilJ. Supercrit. Fluids1998, 12, 1, 59-67. |
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