4,7-DIMETHOXY-1,10-PHENANTHROLINE,97%
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4,7-DIMETHOXY-1,10-PHENANTHROLINE,97%
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CAS No:
92149-07-0
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Formula:
C14H12N2O2
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Chemical Name:
4,7-DIMETHOXY-1,10-PHENANTHROLINE,97%
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Synonyms:
4,7-diMethoxyl-1,10-phenanthroline;4,7-DiMethoxy-1,10-phenanthroline 97%;4,7-Dimethoxy-1,10-phenanthroline ,98%;4,7-DIMETHOXY-1,10-PHENANTHROLINE, 97%;[4,7-DIMETHOXY-1,10-PHENANTHROLINE, 97%]
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CAS No:
Safety Information
UN 3077 9/PG 3
3
22-41-50
26-39-61
Xn: Harmful;N: Dangerous for the environment;
P273-P280-P305 + P351 + P338
H302-H318-H400
|Danger|H302 (97.62%): Harmful if swallowed [Warning Acute toxicity, oral]|P264, P270, P273, P280, P301+P312, P305+P351+P338, P310, P330, P391, and P501|Aggregated GHS information provided by 42 companies from 5 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.
4,7-DIMETHOXY-1,10-PHENANTHROLINE,97% Use and Manufacturing
Under an argon atmosphere, add anhydrous Fe(acac)2 (127.0mg, 0.5mmol) to a 50mL Schlenk flask, and dissolve it in 6mL of anhydrous ethanol at 60 C; Then, a solution of Under an argon atmosphere, add anhydrous Fe(acac)3 (211.8mg, 0.6mmol) to a 50mL Schlenk flask, and dissolve it in 6mL of anhydrous ethanol at 60 C; Then, a solution of General procedure: Dried RuCl3 (0.20 g, 0.96 mmol) was dissolvedin dipropylene glycol (10 mL) and deionized water (1 mL).The solution was refluxed until the metal salt was dissolved, obtaining a dark green solution. Bipyridine (0.469 g; 3.0 mmol) wasadded, resulting in a brown solution. Ascorbic acid (0.177 g, 1.0 mmol) was then added and the solution refluxed for 20 min at250 C, the brown colour changing to red. After cooling, the solutionwas diluted to 40 mL and the pH adjusted to 8 by addition of afew drops of NaOH solution (2.5 M). NaBF4 (4.0 g, 36 mmol) wasadded and the solution cooled on ice. After vacuum filtration, washing with cold water, and drying, 0.329 g [Ru(bpy)3](BF4)2product was obtained.
Computed Properties
Molecular Weight:240.26
XLogP3:2.4
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:240.089877630
Monoisotopic Mass:240.089877630
Topological Polar Surface Area:44.2
Heavy Atom Count:18
Complexity:259
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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4,7-DIMETHOXY-1,10-PHENANTHROLINE,97%
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