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Carbazole-9-ethanol

Carbazole-9-ethanol structure

CAS No:
1484-14-6
Formula:
C14H13NO
Chemical Name:
Carbazole-9-ethanol
Synonyms:
9H-Carbazole-9-ethanol;Carbazole-9-ethanol;N-(2-Hydroxyethyl)carbazole;N-(Hydroxyethyl)carbazole;N-(β-Hydroxyethyl)carbazole;9-(2-Hydroxyethyl)carbazole;2-(9-Carbazolyl)ethanol;2-(N-Carbazolyl)ethanol;NSC 21081;9-(2-Hydroxyethyl)-9H-carbazole;2-(9H-Carbazol-9-yl)ethanol;2-(9H-Carbazol-9-yl)ethan-1-ol
Categories:
Specialty Chemicals

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Carbazole-9-ethanol Basic Attributes

Molecular Weight：

211.264

Exact Mass：

211.26

EC Number：

604-632-3

NSC Number：

21081

DSSTox ID：

DTXSID20281278

HScode：

2933990090

Characteristics

PSA：

25.2

XLogP3：

2.6

Appearance：

Off-white fluffy crystalline powder

Density：

1.17±0.1 g/cm3(Predicted)

Melting Point：

79.5-80.5 °C

Boiling Point：

220 °C @ Press: 5 Torr

Flash Point：

204.6±26.5 °C

Refractive Index：

1.630

Vapor Pressure：

1.27E-07mmHg at 25°C

Safety Information

Transport codes：

NONH for all modes of transport

wgk germany：

hazard class code：

R36/37/38

safety instructions：

26-36

Marks：

Precautionary statement(s)：

P261-P305 + P351 + P338

Hazard Statements：

H315-H319-H335

GHS Classification：

|Warning|H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]|P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, and P501|Aggregated GHS information provided by 38 companies from 1 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.

Carbazole-9-ethanol Use and Manufacturing

16 g of carbazole, 14 g of sodium hydroxide and 7 ml of purified water were mixed with 80 ml of methyl ethyl ketone and the resultant mixture was heated and refluxed under stirring for 30 minutes. While refluxing the mixture, 13 ml of 2-chloroethanol was dropped therein over 1 hour. After refluxing the resultant mixture for additional 3 hours, 8 g of sodium hydroxide was added thereto. While refluxing the resultant mixture, 13 ml of 2-chloroethanol was dropped thereinto over 1 hour. Next, the resultant mixture was refluxed for 24 hours. Then the reaction mixture was cooled to room temperature by allowing to stand, poured into 3 L of purified water and extracted with ether. After removing the ether with an evaporator, the unreacted carbazole was filtered off. From the viscous reaction mixture thus obtained, N-(2-hydroxyethyl)carbazole was isolated by column chromatography (silica gel/benzene). The yield was 20%.

Computed Properties

Molecular Weight:211.26
XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:211.099714038
Monoisotopic Mass:211.099714038
Topological Polar Surface Area:25.2
Heavy Atom Count:16
Complexity:221
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

Recommended Suppliers of Carbazole-9-ethanol

Shanghai Qyubiotech Co., Ltd. Contact Supplier

CN
5 YRS

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Trader Supplier of Material intermediates,Pharmaceutical intermediates,Functional intermediates

Car-bazole-9-eth-anol

Unit Price: $1 /G FOB

CAS No.: 1484-14-6

Grade: Industrial Grade

Content: 97%

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