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2-AMINO-5-FLUOROACETOPHENONE

2-AMINO-5-FLUOROACETOPHENONE structure

CAS No:
2343-25-1
Formula:
C8H8FNO
Chemical Name:
2-AMINO-5-FLUOROACETOPHENONE
Synonyms:
1-(2-Amino-5-fluorophenyl)ethanone;2-amino-5-fluoroacetophenone;Ethanone, 1-(2-amino-5-fluorophenyl)-;C8H8FNO;1-(2-Amino-5-fluorophenyl)ethan-1-one;5-Fluor-2-amino-acetophenon;5-fluoro-2-amino-acetophenone;2"-Amino-5"-fluoroacetophenone;SCHEMBL9665493;CTK0I7944
Categories:
Pharmaceutical Intermediates > Bulk Drug Intermediates

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2-AMINO-5-FLUOROACETOPHENONE Basic Attributes

Molecular Weight：

153.155

Exact Mass：

153.058990

DSSTox ID：

DTXSID20543909

HScode：

2922399090

Characteristics

PSA：

43.1

XLogP3：

1.9

Density：

1.2±0.1 g/cm3

Melting Point：

64-65 °C

Boiling Point：

264.232ºC at 760 mmHg

Flash Point：

113.6±21.8 °C

Refractive Index：

1.548

Vapor Pressure：

0.01mmHg at 25°C

2-AMINO-5-FLUOROACETOPHENONE Use and Manufacturing

To a solution of compound 3 (5 g, 0.037 mol) in 50 ml_ of THF was added asolution of MeMgBr (50 ml_, 0.147 mol) dropwise at 0°C. After addition, themixture was heated to reflux for 4 hours. The mixture was quenched by additionof 10percent HCI, heated to reflux for another 1hour. The resulting mixture was extracted with EtOAc, washed with brine. Thesolvent was evaporated and the residue was purified with chromatography onsilica gel to afford compound 3a (2.8 g, yield: 50percent).To a solution of compound 3a (1 g, 6.54 mmol) in 10 mL of AcOH was added KNCO(2.65 g, 0.033 mol), then the mixture was kept at room temperature for 30 minthen heated to 60°C overnight. H

Computed Properties

Molecular Weight:153.15
XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:153.058992041
Monoisotopic Mass:153.058992041
Topological Polar Surface Area:43.1
Heavy Atom Count:11
Complexity:160
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

Recommended Suppliers of 2-AMINO-5-FLUOROACETOPHENONE

Hangzhou Royalchem Co.,LTD Contact Supplier

CN
2 YRS

Business licensed

Trader Supplier of Pharmaceutical intermediates

2-Amino-5-fluoroacetophenone RC04093

Unit Price: $1 /KG EXW

CAS No.: 2343-25-1

Grade: Industrial Grade

Content: 99%

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Hangzhou Chungyo Chemicals Co., Ltd. Contact Supplier

CN
3 YRS

Business licensed Certified factory

Manufactory Supplier of Dyes,Textile agent,Medical intermediate,API,Pigments,Basic Chemicals

2-AMINO-5-FLUOROACETOPHENONE

CAS No.: 2343-25-1

Grade: pharmaceutical grade

Content: 98%

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Guide of 2-AMINO-5-FLUOROACETOPHENONE

Basic Attributes
Characteristics
Use and Manufacturing
Computed Properties
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