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1-(6-Methoxy-2-naphthalenyl)-1-propanone

1-(6-Methoxy-2-naphthalenyl)-1-propanone structure

CAS No:
2700-47-2
Formula:
C14H14O2
Chemical Name:
1-(6-Methoxy-2-naphthalenyl)-1-propanone
Synonyms:
1-Propanone,1-(6-methoxy-2-naphthalenyl)-;2′-Propionaphthone,6′-methoxy-;1-(6-Methoxy-2-naphthalenyl)-1-propanone;6-Methoxy-2-propionylnaphthalene;1-(6-Methoxy-2-naphthyl)-1-propanone;2-Methoxy-6-propionylnaphthalene;6′-Methoxy-2′-propionaphthone;2-Propionyl-6-methoxynaphthalene;Promen;Ethyl 6-methoxy-2-naphthyl ketone;6-Methoxynaphth-2-yl ethyl ketone
Categories:
Pharmaceutical Intermediates > Bulk Drug Intermediates

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1-(6-Methoxy-2-naphthalenyl)-1-propanone Basic Attributes

Molecular Weight：

214.26

Exact Mass：

214.26

EC Number：

220-285-7

DSSTox ID：

DTXSID90181493

HScode：

2914509090

Characteristics

PSA：

26.3

XLogP3：

3.3

Appearance：

White crystalline powder

Density：

1.095g/cm3

Melting Point：

109 °C

Boiling Point：

180-185 °C @ Press: 0.3 Torr

Flash Point：

161.6ºC

Refractive Index：

1.594

Vapor Pressure：

7.04E-05mmHg at 25°C

Safety Information

Transport codes：

NONH for all modes of transport

wgk germany：

hazard class code：

R36/37/38

safety instructions：

S26-S37/39

Marks：

Xi:Irritant;

Precautionary statement(s)：

P261-P305 + P351 + P338

Hazard Statements：

H315-H319-H335

GHS Classification：

|Warning|H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]|P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, and P501|Aggregated GHS information provided by 38 companies from 1 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.

Drug Information

MeSH Entry Terms：

6-propionyl-2-methoxynaphthalene

1-(6-Methoxy-2-naphthalenyl)-1-propanone Use and Manufacturing

In the is provided with an agitator, reflux condenser, thermometer, dropping funnel in the reaction container, adding triethylamine to 310 ml, stannous chloride 0.65mol, control the stirring speed 190rpm, reducing the temperature of the solution to 5 °C, β-naphthyl methyl ether is slowly added (2) 0.65mol, adds by drops third amide (3) 0.47mol, dropping time control, in 80 min, maintaining the temperature of the solution reaction 9h, raising the temperature of the solution to 19 °C, standing 22h, the reactants are poured into the 1.8L the mass fraction of 25percent sodium bisulfite solution, control the temperature of the solution in the 5 °C, steam distillation, until completely distilled until the triethylamine, control the stirring speed 130rpm, let solution of natural cooling, solidifying oily substance, filtering, potassium nitrate solution, anhydrous calcium sulfate dehydration, in the mass fraction is 92percent recrystallized in cyclohexane solution, to get the yellow solid 6-methoxy-2-c acyl-naphthaline 85.49g, yield 85percent.

Computed Properties

Molecular Weight:214.26
XLogP3:3.3
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:214.099379685
Monoisotopic Mass:214.099379685
Topological Polar Surface Area:26.3
Heavy Atom Count:16
Complexity:249
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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China Professional Manufacturer Supply Great Quality 6'-Methoxy-2'-propiononaphthone CAS 2700-47-2

CAS No.: 2700-47-2

Grade: Pharmaceutical Grade

Content: 99%

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Guide of 1-(6-Methoxy-2-naphthalenyl)-1-propanone

Basic Attributes
Characteristics
Safety Information
Drug Information
Use and Manufacturing
Computed Properties
Recommended Suppliers
Latest News
Learn More Other Chemicals

1-(6-Methoxy-2-naphthalenyl)-1-propanone

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