Benzenemethanamine, 3-iodo-, hydrochloride (1:1)
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Benzenemethanamine, 3-iodo-, hydrochloride (1:1)
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CAS No:
3718-88-5
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Formula:
C7H8IN.ClH
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Chemical Name:
Benzenemethanamine, 3-iodo-, hydrochloride (1:1)
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Synonyms:
Benzenemethanamine,3-iodo-,hydrochloride (1:1);Benzylamine,m-iodo-,hydrochloride;Benzenemethanamine,3-iodo-,hydrochloride;m-Iodobenzylamine hydrochloride;3-Iodobenzylamine hydrochloride
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CAS No:
Benzenemethanamine, 3-iodo-, hydrochloride (1:1) Basic Attributes
269.51
268.946808
5352277
223-068-5
QMV9MZ6TUU
DTXSID10190663
2921499090
Safety Information
NONH for all modes of transport
3
36/37/38-63-42/43
24/25-36/37/39-26-23-22
Xi,T,Xn
Irritant/Light Sensitive
P261-P280-P305 + P351 + P338-P342 + P311
H315-H317-H319-H334-H335-H361
|Danger|H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]|P201, P202, P261, P264, P271, P272, P280, P281, P285, P302+P352, P304+P340, P304+P341, P305+P351+P338, P308+P313, P312, P321, P332+P313, P333+P313, P337+P313, P342+P311, P362, P363, P403+P233, P405, and P501|Aggregated GHS information provided by 46 companies from 5 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.
Benzenemethanamine, 3-iodo-, hydrochloride (1:1) Use and Manufacturing
2.0 g (5.6 mmol) of (A) and 20mL of absolute ethanol was added. After heating to 60 ° C, a solution of hydrazine hydrate in ethanol (0.42 g, 8.4 mmol of hydrazine hydrate dissolved in 3 mL of absolute ethanol) was gradually added dropwise with stirring. Heat stirring reaction 20min. A yellow precipitate generated. Stirring was stopped. 70° C water bath maintained 2.5h. Cooled to RT and precipitated a lot of yellow. The reaction mixture was acidified by adding 4 mL of 1 mol / L hydrochloric acid solution to the reaction bottle. Stirring 30min. Filtration. Washing the filter residue with a small amount of water; The filtrates were combined. Evaporated to dryness under reduced pressure. Vacuum drying to obtain 0.539 g of a yellow solid (B), yield 35.9percent.
Computed Properties
Molecular Weight:269.51
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:268.94682
Monoisotopic Mass:268.94682
Topological Polar Surface Area:26
Heavy Atom Count:10
Complexity:85
Covalently-Bonded Unit Count:2
Compound Is Canonicalized:Yes
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