Diindeno[1,2,3-cd:1′,2′,3′-lm]perylene
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![Diindeno[1,2,3-cd:1′,2′,3′-lm]perylene structure](https://file.echemi.com/fileManage/upload/canonicalSmiles/20220812/5811009ea73e4f8dbc359d3b82188e07.png "Diindeno[1,2,3-cd:1′,2′,3′-lm]perylene")
Diindeno[1,2,3-cd:1′,2′,3′-lm]perylene
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CAS No:
188-94-3
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Formula:
C32H16
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Chemical Name:
Diindeno[1,2,3-cd:1′,2′,3′-lm]perylene
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Synonyms:
Diindeno[1,2,3-cd:1′,2′,3′-lm]perylene;Periflanthene;Periflanthen;NSC 87529;179414-64-3
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CAS No:
Diindeno[1,2,3-cd:1′,2′,3′-lm]perylene Basic Attributes
400.47
400.47
205-875-4
TQA4WPL7Y8
87529
DTXSID40172139
Diindeno[1,2,3-cd:1′,2′,3′-lm]perylene Use and Manufacturing
In advance the flake raw materials of sodium amide into powder, grinding process should pay attention to prevent sodium sesame absorption;20 g of fluoranthene, 10 g of powdered sodium amide, 60 g of N, N-dimethylacetamide were added to the first reaction vessel, Using nitrogen protection, slowly warming to 164 ± 1.5 , And the mixture was stirred for 10 hours to obtain a mixed solution containing indene perylene in dark blue and black, Heating and heating process kept stirring;The mixed solution containing indene perylene was cooled to 10 ° C, and 60 g of absolute ethanol was slowly added dropwise to the mixed solution containing indene perylene. The temperature of the solution was less than or equal to 20 ° C, and the temperature of the solution to be mixed was not increased , Then slowly add 80g water, resulting in deep red solid precipitation, dripping process temperature ≤ 20 , room temperature stirring 6h, filter, filter cake washed to neutral, Dried at 80 for 6h to obtain 15 g of crude indene perylene, the yield was 75.7percent.After the crude indene perylene was pulverized into a powder, Was added to the second reaction vessel, 150 g of toluene was added, and the mixture was heated to toluene and maintained in a reflux state for 3 hours. The filter cake was dried at 80 ° C for 4 hours to obtain 6 g of the first material in the form of a magenta solid powder in a yield of 40 percent. The content of indene perylene was 96.2percent by liquid phase.The first material was added to the third reaction vessel, 90 g of toluene was added, the mixture was heated to toluene and refluxed for 3 hours. The filter cake was dried at 80C for 4 hours to obtain 2.8 g of a second material having a magenta solid powder , The yield was 46.7percent. The content of indene perylene was determined by liquid chromatography to be 98.4percent.
Computed Properties
Molecular Weight:400.5
XLogP3:3.1
Exact Mass:400.125200510
Monoisotopic Mass:400.125200510
Heavy Atom Count:32
Complexity:1450
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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Diindeno[1,2,3-cd:1′,2′,3′-lm]perylene
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