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2-PyridinecarboxiMidoyl chloride, N-hydroxy- 69716-28-5

Name: 2-PyridinecarboxiMidoyl chloride, N-hydroxy- 69716-28-5
Brand: Orient
SKU: pr2511281341
Price: 4 USD
Availability: InStock

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CAS No.:

69716-28-5

Grade:

Industrial Grade

Content:

98%

Port:

SHAGNHAI

Brand:

Orient

Packaging:

1KG, 25KG, 200KG, 1000KG, customized

Price valid (until):

2025-12-28

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Qingdao Orient Chemical Co.,LTD

Company Type:

Trader

Location:

China

Qualification:

Main Products:

pharmaceutical intermediates,peptides,electronic chemicals

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Product Description
Seller Information

Description

Focusing on innovative research, development, and production in the field of fine chemicals, we prioritize technology, quality, and market orientation. We collaborate with global partners to build a high-tech chemical industry chain and promote sustainable development in the industry.

The company's main products include pharmaceutical intermediates, food additives, essence, spices and plant extracts. The products have passed international certification and are exported to Europe, America, Japan, South Korea and Southeast Asia.

Product Name:

4-(Aminomethyl)-1-methyl-piperidin-4-ol

Synonyms:

4-(aminomethyl)-1-methylpiperidin-4-ol dihydrochloride;4-piperidinol, 4-(aminomethyl)-1-methyl-;4-Aminomethyl-1-methylpiperidin-4-ol;4-(aminomethyl)-1-methylpiperidin-4-ol(SALTDATA: 2HCl);4-aMinoMethyl-4-hydroxy-1-Methylpiperidine(HCl)

CAS:

26228-68-2

MF:

C7H16N2O

MW:

144.21

EINECS:

Product Categories:

Mol File:

26228-68-2.mol

2-PyridinecarboxiMidoyl chloride, N-hydroxy- Basic information

Product Name:	2-PyridinecarboxiMidoyl chloride, N-hydroxy-
Synonyms:	2-PyridinecarboxiMidoyl chloride, N-hydroxy-;(Z)-N-HydroxypicoliniMidoyl chloride;N-Hydroxy-2-pyridinecarboximidoyl chloride;Pyridine-2-carbohydroximoyl chloride;N-Hydroxypicolinimidoyl chloride;(Z)-N-Hydroxypyridine-2-carbonimidoyl chloride;2-[chloro(nitroso)methylidene]-1H-pyridine
CAS:	69716-28-5
MF:	C6H5ClN2O
MW:	156.57
EINECS:
Product Categories:
Mol File:	69716-28-5.mol

2-PyridinecarboxiMidoyl chloride, N-hydroxy- Chemical Properties

Melting point	144℃ (benzene )
density	1.34±0.1 g/cm3 (20 ºC 760 Torr)
storage temp.	under inert gas (nitrogen or Argon) at 2-8°C

2-PyridinecarboxiMidoyl chloride, N-hydroxy- Usage And Synthesis

Synthesis Reference(s)	Synthetic Communications, 18, p. 1427, 1988 DOI: 10.1080/00397918808078813
Synthesis	873-69-8 69716-28-5 2-Pyridine carboxaldehyde oxime (288a, 180 mg, 1.47 mmol) was used as raw material and dissolved in DMF (2 mL) at 20 °C. Subsequently, N-chlorosuccinimide (NCS, 216 mg, 1.62 mmol) was added all at once. The reaction mixture was stirred at 20 °C for 12 hours. After completion of the reaction, the mixture was concentrated. The residue was poured into water (20 mL) and the aqueous phase was extracted with ethyl acetate (50 mL × 3). The combined organic phases were washed with brine (20 mL × 2), dried over anhydrous Na2SO4, filtered and concentrated in vacuo to afford 2-pyridine carboxaldehyde oxime chloride (288b, 200 mg, yield: 87.1%) as a brown solid.1H NMR (400 MHz, CDCl3) δ 10.79 (br s, 1H), 8.72 (d, J = 4.2 Hz, 1H) , 7.94 (d, J = 8.2 Hz, 1H), 7.80 (dt, J = 1.7, 7.8 Hz, 1H), 7.39 (ddd, J = 0.8, 5.0, 7.4 Hz, 1H), 2.79 (s, 1H).
References	[1] Patent: WO2018/64119, 2018, A1. Location in patent: Paragraph 1352 [2] Patent: WO2008/23248, 2008, A2. Location in patent: Page/Page column 94 [3] Patent: US2009/247478, 2009, A1. Location in patent: Page/Page column 50 [4] Patent: WO2012/76989, 2012, A1. Location in patent: Page/Page column 52 [5] Tetrahedron, 2000, vol. 56, # 8, p. 1057 - 1064

4-(Aminomethyl)-1-methyl-piperidin-4-ol Chemical Properties

Boiling point	255.7±15.0 °C(Predicted)
density	1.047±0.06 g/cm3(Predicted)
pka	12.55±0.20(Predicted)

Safety Information

Hazard Codes	Xn
Risk Statements	22

First-aid measures

If inhaled

Move the victim into fresh air. If breathing is difficult, give oxygen. If not breathing, give artificial respiration and consult a doctor immediately. Do not use mouth to mouth resuscitation if the victim ingested or inhaled the chemical.

Following skin contact

Take off contaminated clothing immediately. Wash off with soap and plenty of water. Consult a doctor.

Following eye contact

Rinse with pure water for at least 15 minutes. Consult a doctor.

Following ingestion

Rinse mouth with water. Do not induce vomiting. Never give anything by mouth to an unconscious person. Call a doctor or Poison Control Center immediately.

Accidental release measures

Personal precautions, protective equipment and emergency procedures

Avoid dust formation. Avoid breathing mist, gas or vapours.Avoid contacting with skin and eye. Use personal protective equipment.Wear chemical impermeable gloves. Ensure adequate ventilation.Remove all sources of ignition. Evacuate personnel to safe areas.Keep people away from and upwind of spill/leak.

Environmental precautions

Prevent further spillage or leakage if it is safe to do so. Do not let the chemical enter drains. Discharge into the environment must be avoided.

Methods and materials for containment and cleaning up

Collect and arrange disposal. Keep the chemical in suitable and closed containers for disposal. Remove all sources of ignition. Use spark-proof tools and explosion-proof equipment. Adhered or collected material should be promptly disposed of, in accordance with appropriate laws and regulations.

Handling and storage

Precautions for safe handling

Handling in a well ventilated place. Wear suitable protective clothing. Avoid contact with skin and eyes. Avoid formation of dust and aerosols. Use non-sparking tools. Prevent fire caused by electrostatic discharge steam.

Conditions for safe storage, including any incompatibilities

Store the container tightly closed in a dry, cool and well-ventilated place. Store apart from foodstuff containers or incompatible materials

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—— Q&A ——

Q1:Do you provide sample?

A: Yes, we can provide free sample, you only need pay the shipping cost.

Q2: What is the lead time?

A: For stock goods, it usually take about 5-7 days by air, 15-30 days by sea,For customized products, the delivery time needs to be confirmed based on the actual situation.

Q3: How can I buy? What is the payment method?

A: You can contract us through Email or you can browse our website:orientchem.cc, we have bank transfer,

A：We attach great importance to after-sales service of our products. If there are any quality issues, please contact us within 30 days of receiving the goods and we will handle returns and exchanges for you.

Certificates

Basic Info

Product Name:

N-hydroxypyridine-2-carboximidoyl chloride

Other Name:

N-Hydroxypicolinimidoyl chloride;69716-28-5;2-[chloro(nitroso)methylidene]-1H-pyridine;pyridine hydroximoyl chloride;ON=C(Cl)C1=CC=CC=N1;pyridine-2-carbohydroximoyl chloride;ANW-61272;AK-50047;N-hydroxy-2-pyridinecarboximidoyl chloride;FT-0687580;(2E)-2-[chloro(nitroso)methylidene]-1H-pyridine

CAS No.:

69716-28-5

Molecular Formula:

C6H5ClN2O

InChIKeys:

XBTPHBYKYXWYOZ-UHFFFAOYSA-N

Molecular Weight:

156.57 g/mol

Exact Mass:

156.0090405 g/mol

DSSTox ID:

DTXSID60425437

Categories:

Bulk Drug Intermediates

Characteristics

PSA:

45.5 Å²

See More N-hydroxypyridine-2-carboximidoyl chloride Properties 

Seller Information

Business Type:
Trader

Main Products:
pharmaceutical intermediates,peptides,electronic chemicals

Location:
Room 102, 1st Floor, East Office Building, No. 45 Pengwan Road, Qianwan Bonded Port Area, Qingdao Zone, China (Shandong) Pilot Free Trade Zone

Payment Terms:
100% TT in advance

Average lead Time:
10

Total Annual Revenue:
$10 million-$25 million

Total Employees:
51-100

Year of Establishment:
2024

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We are mainly specilized in supply of pharmaceutical intermediates, electronic chemicals，food additives, and other fine chemical products.
Integrity is the foundation, quality is life. We would like to work together with you to build a greener and brighter future.

Website: orientchem.cc
Email: scarlett@orientchem.cc
WhatsApp: +86 17753254221
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