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METHYL 2-AMINO-5-BROMO-4-PYRIDINECARBOXYLATE

METHYL 2-AMINO-5-BROMO-4-PYRIDINECARBOXYLATE structure

CAS No:
882499-87-8
Formula:
C7H7BrN2O2
Chemical Name:
METHYL 2-AMINO-5-BROMO-4-PYRIDINECARBOXYLATE
Synonyms:
METHYL 2-AMINO-5-BROMO-4-PYRIDINECARBOXYLATE;METHYL 2-AMINO-5-BROMOPYRIDINE-4-CARBOXYLATE;METHYL 2-AMINO-5-BROMOISONICOTINATE;Methyl 2-amino-5-bromoisonicotinate 98%;Methyltinate 2-amino-5-bromoisonico;Methyl 2-amino-5-bromopyridine-4-carboxylate, 2-Amino-5-bromo-4-(methoxycarbonyl)pyridine;2-AMino-5-broMoisonicotinic acid Methyl ester;4-Pyridinecarboxylic acid, 2-aMino-5-broMo-, Methyl ester
Categories:
Pharmaceutical Intermediates > Heterocyclic Compound

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METHYL 2-AMINO-5-BROMO-4-PYRIDINECARBOXYLATE Basic Attributes

Molecular Weight：

231.04668

Exact Mass：

229.969086

EC Number：

1533716-785-6

DSSTox ID：

DTXSID20649576

HScode：

2933399090

Characteristics

PSA：

65.2

XLogP3：

Density：

1.7±0.1 g/cm3

Boiling Point：

311.5°C at 760 mmHg

Flash Point：

142.2±26.5 °C

Refractive Index：

1.608

Safety Information

Hazard category：

IRRITANT

Marks：

Hazard note：

Irritant

Precautionary statement(s)：

P261, P272, P280, P302+P352, P321, P333+P313, P363, P501

Hazard Statements：

H317

GHS Classification：

|Warning|H317 (100%): May cause an allergic skin reaction [Warning Sensitization, Skin]|P261, P272, P280, P302+P352, P321, P333+P313, P363, and P501|Aggregated GHS information provided by 39 companies from 1 notifications to the ECHA C&L Inventory.

METHYL 2-AMINO-5-BROMO-4-PYRIDINECARBOXYLATE Use and Manufacturing

Step 15.1 : 2-Amino-5-bromo-isonicotinic acid methyl ester.A solution of 2-amino-isonicotinic acid methyl ester (5.58 g, 36.7 mmol) in DMF (56 mL) was cooled to -18°C (ice / MeOH bath), treated with NBS (7.21 g, 38.5 mmol), and stirred at - 18°C for 1 h. The reaction mixture was diluted in AcOEt (500 mL) and washed with water (2 x 250 mL). The organic layer was dried over Na2-Amino-5-bromo-isonicotinic acid methyl ester; Bromine (1.78 ml, 34.8 mmol) was added dropwise over an hour to a stirred solution of 2-amino-isonicotinic acid methyl ester (5.13 g, 33.75 mmol) in chloroform (350 ml) at room temperature and the orange solution stirred at room temperature overnight. A 2N solution of sodium thiosulfate (300 ml) was added to the reaction and stirred for ten minutes. The two layers were separated and the aqueous extracted with chloroform (100 ml). The combined organics were dried (MgSO

Computed Properties

Molecular Weight:231.05
XLogP3:1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:229.96909
Monoisotopic Mass:229.96909
Topological Polar Surface Area:65.2
Heavy Atom Count:12
Complexity:177
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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Factory Price METHYL 2-AMINO-5-BROMO-4-PYRIDINECARBOXYLATE 882499-87-8

CAS No.: 882499-87-8

Grade: Pharmaceutical Grade

Content: 99%

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Guide of METHYL 2-AMINO-5-BROMO-4-PYRIDINECARBOXYLATE

Basic Attributes
Characteristics
Safety Information
Use and Manufacturing
Computed Properties
Recommended Suppliers
Latest News
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METHYL 2-AMINO-5-BROMO-4-PYRIDINECARBOXYLATE

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