 Home > Encyclopedia > 4-Iodobenzyl bromide

4-Iodobenzyl bromide

4-Iodobenzyl bromide structure

CAS No:
16004-15-2
Formula:
C7H6BrI
Chemical Name:
4-Iodobenzyl bromide
Synonyms:
Benzene,1-(bromomethyl)-4-iodo-;Toluene,α-bromo-p-iodo-;1-(Bromomethyl)-4-iodobenzene;p-Iodobenzyl bromide;4-Iodobenzyl bromide;α-Bromo-p-iodotoluene
Categories:
Organic Chemistry > Hydrocarbons and Derivatives

Request for Quotation

Description

light yellow adhering crystalline powder

4-Iodobenzyl bromide Basic Attributes

Molecular Weight：

296.93

Exact Mass：

296.93

BRN：

2325160

EC Number：

700-046-8

DSSTox ID：

DTXSID40359261

HScode：

29039990

Characteristics

PSA：

XLogP3：

Appearance：

Light yellow Adhering Crystalline Powder

Density：

2.0672 (rough estimate)

Melting Point：

84.5-85.0 °C

Boiling Point：

200-205 °C @ Press: 4 Torr

Flash Point：

140°C/15mm

Refractive Index：

1.6500 (estimate)

Water Solubility：

Insoluble in water.

Storage Conditions：

2-8°C

Vapor Pressure：

0.0202mmHg at 25°C

Safety Information

Packing level：

Ⅱ

Hazard category：

Transport codes：

UN 3261 8/PG 2

wgk germany：

hazard class code：

34-63-42/43-36/37/38

safety instructions：

26-36/37/39-45-23

Marks：

C,T

Hazard note：

Corrosive/Lachrymatory/Light Sensitive

Precautionary statement(s)：

P280-P305 + P351 + P338-P310

Hazard Statements：

H314

GHS Classification：

|Danger|H314 (99.28%): Causes severe skin burns and eye damage [Danger Skin corrosion/irritation]|P260, P264, P280, P301+P330+P331, P303+P361+P353, P304+P340, P305+P351+P338, P310, P321, P363, P405, and P501|Aggregated GHS information provided by 140 companies from 8 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.

4-Iodobenzyl bromide Use and Manufacturing

Synthesis of Compound 1D [0026] p-Iodotoluene (Compound 1C, 25 g), N-bromosuccinimide (23.5 g) and benzoyl peroxide (375 mg) were added to carbon tetrachloride (375 ml) and refluxed with heating for 7 hours under photoirradiation. Further, the reaction mixture was stirred overnight at room temperature, then insoluble matters were removed by filtration, and the filtrate was concentrated under reduced pressure. The concentrated residue was recrystallized from ethyl acetate and hexane to obtain Compound 1D (yield: 60.3percent). [0027] NMR chemical shift, CDCl3, TMS as standard [0028] d 7.72 (d, 2H), 7.14 (d, 2H), 4.39 (s, 2H)Step 1

Computed Properties

Molecular Weight:296.93
XLogP3:4
Rotatable Bond Count:1
Exact Mass:295.86976
Monoisotopic Mass:295.86976
Heavy Atom Count:9
Complexity:77
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

Recommended Suppliers of 4-Iodobenzyl bromide

HANGZHOU LEAP CHEM CO., LTD. Contact Supplier

CN
5 YRS

Business licensed

Trader Supplier of Intermediates,Building blocks,API,Silicones,Peptides,Lab chemicals,Biochemicals,Pharmaceuticals,Screening Compounds,Food Additives

4-Iodobenzyl bromide

CAS No.: 16004-15-2

Content: 99.00%

Inquiry