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N-Methyl-3-pyridinamine

N-Methyl-3-pyridinamine structure

CAS No:
18364-47-1
Formula:
C6H8N2
Chemical Name:
N-Methyl-3-pyridinamine
Synonyms:
METHYL-PYRIDIN-3-YL-AMINE;3-METHYLAMINOPYRIDINE;n-methyl-3-pyridinamine;3-Pyridinamine,N-methyl-;3-AMINOMETHYL PYRIDINE 97%;methyl(3-pyridyl)amine;N-methylpyridin-3-amine;N-methyl-N-(3-pyridyl)amine
Categories:
Pharmaceutical Intermediates > Heterocyclic Compound

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Description

Liquid

N-Methyl-3-pyridinamine Basic Attributes

Molecular Weight：

108.14

Exact Mass：

108.068748

UNII：

33VNV59XC6

DSSTox ID：

DTXSID70171458

HScode：

29333990

Characteristics

PSA：

24.9

XLogP3：

0.8

Appearance：

Yellow Liquid

Density：

1.06g/ml

Melting Point：

201 °C

Boiling Point：

110°C/7mmHg(lit.)

Flash Point：

82.8±19.8 °C

Refractive Index：

1.5840 to 1.5880

Vapor Pressure：

0.165mmHg at 25°C

Safety Information

Hazard category：

6.1

hazard class code：

safety instructions：

36/37

Precautionary statement(s)：

P264, P280, P302+P352, P305+P351+P338, P321, P332+P313, P337+P313, P362

Hazard Statements：

H315

GHS Classification：

|Warning|H227 (33.33%): Combustible liquid [Warning Flammable liquids]|P210, P261, P264, P270, P271, P280, P301+P312, P302+P352, P304+P312, P304+P340, P305+P351+P338, P312, P321, P322, P330, P332+P313, P337+P313, P362, P363, P370+P378, P403+P233, P403+P235, P405, and P501|Aggregated GHS information provided by 3 companies from 2 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.

N-Methyl-3-pyridinamine Use and Manufacturing

Stage 1Methylpyridin-3-ylamine An amount of 100.1 g (633 mmol) of 3-bromopyridine was stirred with 160 ml (1280 mmol) of 8M methylamine in ethanol, 4 g (27.5 mmol) of 8-hydroxyquinoline and 2.2 g (11.5 mmol) of copper(I) iodide in an autoclave at 120° for 16 hours. The mixture was filtered with suction over sand/silica gel and concentrated, aqueous citric acid and cyclohexane were added to the residue, the aqueous phase was saturated with sodium chloride, admixed with dilute aqueous sodium hydroxide solution to a pH of 10 and extracted 6 times with ethyl acetate, and the combined organic phases were dried over MgSO

Computed Properties

Molecular Weight:108.14
XLogP3:0.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:108.068748264
Monoisotopic Mass:108.068748264
Topological Polar Surface Area:24.9
Heavy Atom Count:8
Complexity:63.5
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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N-Methyl-3-pyridinamine

CAS No.: 18364-47-1

Content: 99.00%

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Tianjin Jinshu Technology Co., Ltd. Contact Supplier

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CAS No.: 18364-47-1

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Content: 99%

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