2-amino-N,N-dimethylacetamide
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2-amino-N,N-dimethylacetamide
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CAS No:
1857-19-8
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Formula:
C4H10N2O
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Chemical Name:
2-amino-N,N-dimethylacetamide
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Synonyms:
N,N-Dimethyl-2-aminoacetamide;2-diazenyl-N,N-dimethylacetamide;2-Amino-N,N-dimethylacetamide;Glycine dimethylamide, 97%;A80236;N~1~,N~1~-dimethylglycinamide(SALTDATA: HCl);N~1~,N~1~-dimethylglycinamide 1HCl;2-aMino-N,N-diMethylacetaMide hcl
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CAS No:
Characteristics
46.3
-1.2
0.995±0.06 g/cm3(Predicted)
60 °C(Press: 0.8 Torr)
63.5±22.6 °C
1.455
0.856mmHg at 25°C
2-amino-N,N-dimethylacetamide Use and Manufacturing
General procedure: This procedure is illustrated for compound 11a. To a solution of compound 10a (170 mg, 0.77 mmol) in methanol (10 mL), 10percent Pd/C was added. The reaction was hydrogenated at room temperature and atmospheric pressure for 3 h. Then the catalyst was filtered off through Celite, and the clear solution, taken to dryness, afforded the title compound as an oil. The reaction was monitored by TLC and, for stability problems, the amine was directly used in the subsequent reaction. Yield 97percent.General procedure: This procedure is illustrated for compound 11a. To a solution of compound 10a (170 mg, 0.77 mmol) in methanol (10 mL), 10percent Pd/C was added. The reaction was hydrogenated at room temperature and atmospheric pressure for 3 h. Then the catalyst was filtered off through Celite, and the clear solution, taken to dryness, afforded the title compound as an oil. The reaction was monitored by TLC and, for stability problems, the amine was directly used in the subsequent reaction. Yield 97percent.
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