6-broMo-3-iodoH-iMidazo[1,2-a]pyridine
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![6-broMo-3-iodoH-iMidazo[1,2-a]pyridine structure](https://file.echemi.com/fileManage/upload/canonicalSmiles/20220811/d8cbc840ed8d4ecd89b46a360871cb16.png "6-broMo-3-iodoH-iMidazo[1,2-a]pyridine")
6-broMo-3-iodoH-iMidazo[1,2-a]pyridine
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CAS No:
474706-74-6
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Formula:
C6H4BrIN2O
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Chemical Name:
6-broMo-3-iodoH-iMidazo[1,2-a]pyridine
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Synonyms:
6-Bromo-3-iodoimidazo[1,2-a]pyridine;6-bromo-3-iodoH-imidazo[1,2-a]pyridine;Imidazo[1,2-a]pyridine, 6-bromo-3-iodo-;SCHEMBL381224;CTK8B5242;DTXSID90621809;KS-00000PM6;ANW-48103;MFCD18800553;SC4328
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Safety Information
|Warning|H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]|P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, and P501|The GHS information provided by 1 company from 1 notification to the ECHA C&L Inventory.
6-broMo-3-iodoH-iMidazo[1,2-a]pyridine Use and Manufacturing
To a solution of 6-bromoimidazo[1, 2-a]pyridine (721 mg 3.66 mmol) in 20 mL ACN were added 988 mg (4.39 mmol) of N-iodosuccinimide. The reaction was stirred at room temperature for 1 h. Solvent was removed in vacuo then residue was diluted with CHTo a slightly cloudy mixture of 6-bromoimidazo[l, 2-α]pyridine (15.4 g, 78.0 mmol) in dry MeCN (500 mL) was added jV-iodosuccinimide (17.6 g, 78.0 mmol) portionwise over ~5 min (a precipitate immediately formed). After 16 h, the crude product was collected by filtration and triturated with boiling MeCN to provide 19.56 g (77percent) of the title compound as an off-white solid. MS(ES)+ m/e 198.7 [M+H]Step: 1 To a solution of 6-bromoimidazo [l , 2-a]pyridine (20 g, 101.5 mmol) in ACN (300 mL) was added N-iodosuccinimide (22.8 g, 101.5 mmol) at rt and stirred for 5 h. The reaction mixture was filtered and washed with hot acetonitrile to afford 6-bromo-3-iodoimidazo[l, 2- ajpyridine (22 g, 67percent) as a pale yellow solid. 1H NMR (400 MHz, CDC1To a solution of 6-bromoimidazo[1, 2-a]pyridine (20 g, 101.5 mmol) in ACN (300 mL) was added N-iodosuccinimide (22.8 g, 101.5 mmol) at rt and stirred for 5 h. To a solution of 6-bromoimidazo[1, 2-a]pyridine (5 g, 25.4 mmol) in CH
Computed Properties
Molecular Weight:322.93
XLogP3:3.1
Hydrogen Bond Acceptor Count:1
Exact Mass:321.86026
Monoisotopic Mass:321.86026
Topological Polar Surface Area:17.3
Heavy Atom Count:11
Complexity:155
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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6-broMo-3-iodoH-iMidazo[1,2-a]pyridine
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