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2-BROMO-3-PHENYLPYRIDINE

2-BROMO-3-PHENYLPYRIDINE structure

CAS No:
32864-29-2
Formula:
C11H8BrN
Chemical Name:
2-BROMO-3-PHENYLPYRIDINE
Synonyms:
2-bromo-3-phenylpyridine;Pyridine,2-bromo-3-phenyl-;Pyridine, 2-bromo-3-phenyl-;SCHEMBL1203598;CTK4G9467;DTXSID70376466;ZINC14982294;DS-4353;QC-4987;VP14203
Categories:
Chemical Reagents > Organic Reagents

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2-BROMO-3-PHENYLPYRIDINE Basic Attributes

Molecular Weight：

234.09

Exact Mass：

232.98400

DSSTox ID：

DTXSID70376466

HScode：

2933399090

Characteristics

PSA：

12.9

XLogP3：

3.5

Density：

1.426 g/cm3

Flash Point：

148.1ºC

Refractive Index：

1.606

2-BROMO-3-PHENYLPYRIDINE Use and Manufacturing

General procedure: In a 1 L reaction vessel Intermediate A-3 (25 g), Phenylboronic acid (10.74 g), & lt; RTI ID = 0.0 & gt; Pd (PPh3) 4 (3.05 g), K2CO3 (24.3 g) , THF (333 mL) and distilled water (166 mL) were put together, And refluxed under nitrogen for 12 hours. After completion of the reaction, the reaction mixture was cooled to room temperature, and the aqueous layer was removed. The organic layer was washed with 5% brine (500 mL) And once with distilled water (500 mL). The organic layer obtained was dried over MgSO4, the solvent was removed, and ethyl acetate: n-hexane (= 3: 97) The residue was purified by silica gel column chromatography Purification yielded intermediate A-2 (12.4 g).

Computed Properties

Molecular Weight:234.09
XLogP3:3.5
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:232.98401
Monoisotopic Mass:232.98401
Topological Polar Surface Area:12.9
Heavy Atom Count:13
Complexity:154
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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CAS No.: 32864-29-2

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32864-29-2 2-bromo-3-phenylpyridine

CAS No.: 32864-29-2

Grade: Industrial Grade

Content: 95%

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