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Home > Encyclopedia > 3,3′-[[4-[2-(2,6-Dichloro-4-nitrophenyl)diazenyl]phenyl]imino]bis[propanenitrile]

3,3′-[[4-[2-(2,6-Dichloro-4-nitrophenyl)diazenyl]phenyl]imino]bis[propanenitrile]

3,3′-[[4-[2-(2,6-Dichloro-4-nitrophenyl)diazenyl]phenyl]imino]bis[propanenitrile] structure

3,3′-[[4-[2-(2,6-Dichloro-4-nitrophenyl)diazenyl]phenyl]imino]bis[propanenitrile] 

structure
  • CAS No:

    67923-43-7

  • Formula:

    C18H14Cl2N6O2

  • Chemical Name:

    3,3′-[[4-[2-(2,6-Dichloro-4-nitrophenyl)diazenyl]phenyl]imino]bis[propanenitrile]

  • Synonyms:

    Propanenitrile,3,3′-[[4-[2-(2,6-dichloro-4-nitrophenyl)diazenyl]phenyl]imino]bis-;Propanenitrile,3,3′-[[4-[(2,6-dichloro-4-nitrophenyl)azo]phenyl]imino]bis-;Propionitrile,3,3′-[p-(2,6-dichloro-4-nitrophenylazo)phenylimino]di-;3,3′-[[4-[2-(2,6-Dichloro-4-nitrophenyl)diazenyl]phenyl]imino]bis[propanenitrile];Disperse Yellow 163;C.I. 111235;C.I. Disperse Yellow 163;Kayalon Polyester Yellow BRL-S;Kiwalon Polyester Yellow BRF;71767-67-4

  • Categories:

    Pharmaceutical Intermediates  >  Bulk Drug Intermediates

Description

DryPowder

3,3′-[[4-[2-(2,6-Dichloro-4-nitrophenyl)diazenyl]phenyl]imino]bis[propanenitrile] Basic Attributes

417.24876

417.25

267-758-4

DTXSID7070846

Characteristics

121

6.47396

DryPowder

1.37

685.4ºC at 760 mmHg

368.3ºC

1.64

Safety Information

P261, P272, P280, P302+P352, P321, P333+P313, P363, P501

H317

|Warning|H317 (100%): May cause an allergic skin reaction [Warning Sensitization, Skin]|P261, P272, P280, P302+P352, P321, P333+P313, P363, and P501|Aggregated GHS information provided by 15 companies from 2 notifications to the ECHA C&L Inventory.

3,3′-[[4-[2-(2,6-Dichloro-4-nitrophenyl)diazenyl]phenyl]imino]bis[propanenitrile] Use and Manufacturing

Methods of Manufacturing

Using 2, 6-dichloro-4-nitroaniline and N, N-dicyanoethylaniline as raw materials, first diazotize the former and then couple with the latter to obtain the product. After filtering, grinding and drying, the finished product is obtained. . Add 98% sulfuric acid to the diazotization pot, lower the temperature to below 10°C, slowly add the dried and crushed sodium nitrite, increase the temperature to 70°C, keep it for 30 minutes, then lower the temperature to 0-10°C, and slowly add 2 , 6-Dichloro-4-nitroaniline, after the addition, continue to stir and react for 4h to obtain diazonium liquid. The feeding ratio of each reactant: 2, 6-dichloro-4-nitroaniline: sulfuric acid: sodium nitrite=1:1.5:1.03 (the ratio of the amount of substances). In the coupling pot, add the diazonium liquid in a trickle into 2 times its mass of crushed ice to dilute, and then slowly add N, N-dicyanoethyl aniline dissolved in 40% sulfuric acid to maintain 5-10℃ After the addition, continue to stir for 10h, then heat to 50-55℃ and stir for more than 5h, press filte

Uses

Disperse yellow BR is suitable for dyeing and printing polyester and blended fabrics.


Dyes


Fabric, textile, and leather products not covered elsewhere

Production

25,000 - 100,000 lb

Textiles, apparel, and leather manufacturing|Propanenitrile, 3,3'-[[4-[2-(2,6-dichloro-4-nitrophenyl)diazenyl]phenyl]imino]bis-: ACTIVE

Computed Properties

Molecular Weight:417.2
XLogP3:4.3
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:7
Exact Mass:416.0555291
Monoisotopic Mass:416.0555291
Topological Polar Surface Area:121
Heavy Atom Count:28
Complexity:611
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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