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Disperse Yellow 163

Disperse Yellow 163 structure

CAS No:
67923-43-7
Formula:
C18H14Cl2N6O2
Chemical Name:
Disperse Yellow 163
Synonyms:
3,3'-[[4-[(2,6-dichloro-4-nitrophenyl)azo]phenyl]imino]bispropiononitrile;C.I. Disperse Yellow 163 press cake;3,3'-[[4-[(2,6-Dichloro-4-nitrophenyl)azo]phenyl]imino]bispropanenitrile;C.I. 111235;Disperse Yellow 163;Allilon Yellow S-BRL;Disperse Yellow BR;Hisperse Yellow C-BR
Categories:
Pharmaceutical Intermediates > Bulk Drug Intermediates

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Description

DryPowder

Disperse Yellow 163 Basic Attributes

Molecular Weight：

417.25

Exact Mass：

417.25

EC Number：

267-758-4

TSCA：

TSCA listed

DSSTox ID：

DTXSID7070846

Characteristics

PSA：

121

XLogP3：

6.47396

Appearance：

DryPowder

Density：

1.37

Boiling Point：

685.4±55.0 °C(Predicted)

Flash Point：

368.3ºC

Refractive Index：

1.64

Flammability characteristics：

Not classified

PKA：

0.86±0.50(Predicted)

Safety Information

Precautionary statement(s)：

P261, P272, P280, P302+P352, P321, P333+P313, P363, P501

Hazard Statements：

H317

GHS Classification：

|Warning|H317 (100%): May cause an allergic skin reaction [Warning Sensitization, Skin]|P261, P272, P280, P302+P352, P321, P333+P313, P363, and P501|Aggregated GHS information provided by 15 companies from 2 notifications to the ECHA C&L Inventory.

Disperse Yellow 163 Use and Manufacturing

Methods of Manufacturing

Using 2, 6-dichloro-4-nitroaniline and N, N-dicyanoethylaniline as raw materials, first diazotize the former and then couple with the latter to obtain the product. After filtering, grinding and drying, the finished product is obtained. . Add 98% sulfuric acid to the diazotization pot, lower the temperature to below 10°C, slowly add the dried and crushed sodium nitrite, increase the temperature to 70°C, keep it for 30 minutes, then lower the temperature to 0-10°C, and slowly add 2 , 6-Dichloro-4-nitroaniline, after the addition, continue to stir and react for 4h to obtain diazonium liquid. The feeding ratio of each reactant: 2, 6-dichloro-4-nitroaniline: sulfuric acid: sodium nitrite=1:1.5:1.03 (the ratio of the amount of substances). In the coupling pot, add the diazonium liquid in a trickle into 2 times its mass of crushed ice to dilute, and then slowly add N, N-dicyanoethyl aniline dissolved in 40% sulfuric acid to maintain 5-10℃ After the addition, continue to stir for 10h, then heat to 50-55℃ and stir for more than 5h, press filte

Uses

Disperse yellow BR is suitable for dyeing and printing polyester and blended fabrics.

Dyes

Fabric, textile, and leather products not covered elsewhere

Production

25,000 - 100,000 lb

Manufacturing Info：

Textiles, apparel, and leather manufacturing|Propanenitrile, 3,3'-[[4-[2-(2,6-dichloro-4-nitrophenyl)diazenyl]phenyl]imino]bis-: ACTIVE

Computed Properties

Molecular Weight:417.2
XLogP3:4.3
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:7
Exact Mass:416.0555291
Monoisotopic Mass:416.0555291
Topological Polar Surface Area:121
Heavy Atom Count:28
Complexity:611
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes