3,8-Dibromophenanthroline
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3,8-Dibromophenanthroline
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CAS No:
100125-12-0
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Formula:
C12H8Br2N2
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Chemical Name:
3,8-Dibromophenanthroline
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Synonyms:
3,8-Dibromo-1,10-phenanthroline;3,8-Dibromophenanthroline;3,8-Dibromophenanthr;1,10-Phenanthroline,3,8-dibroMo-;3,8-dibromo-1,7-phenanthroline;3,8-Dibromophenthroline
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CAS No:
Characteristics
25.8
3.8
1.915
221-222 °C
428.9±40.0 °C(Predicted)
213.2±27.3 °C
1.772
0mmHg at 25°C
Safety Information
|Warning|H302 (100%): Harmful if swallowed [Warning Acute toxicity, oral]|P261, P264, P270, P271, P280, P301+P312, P302+P352, P304+P312, P304+P340, P305+P351+P338, P312, P321, P330, P332+P313, P337+P313, P362, P403+P233, P405, and P501|The GHS information provided by 1 company from 1 notification to the ECHA C&L Inventory.
3,8-Dibromophenanthroline Use and Manufacturing
In a 500 ml bottle of the, adding 200mL1-chlorobutane, 1, 10-O-phenan throline 5g in other words 27.8mmol, S1, 10-phenanthroline (5 g, 27.8mmol), S2Cl2 (12.3 g, 91.1mmol), pyridine (7.10 g, 89.8mmol), Br2 (14 g, 87.6 mmol) in 1-chlorobutane (200 mL) and the mixture 12 heating time, the mixture was stirred. After the reaction was completed, a solid produced was separated lowering to room temperature. It was added an excess of NaOH and extracted with dichloro-menthane with water and dried over MgSO4. SiO2 column and recrystallized with dichloromethane to obtain the compound 1-A (5.9 g).
Computed Properties
Molecular Weight:338.00
XLogP3:3.8
Hydrogen Bond Acceptor Count:2
Exact Mass:337.88772
Monoisotopic Mass:335.88977
Topological Polar Surface Area:25.8
Heavy Atom Count:16
Complexity:235
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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