2-(4-METHYLPIPERAZINO)-3-PYRIDINAMINE
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2-(4-METHYLPIPERAZINO)-3-PYRIDINAMINE
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CAS No:
5028-17-1
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Formula:
C10H16N4
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Chemical Name:
2-(4-METHYLPIPERAZINO)-3-PYRIDINAMINE
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Synonyms:
AKOSB034160;2-(4-METHYLPIPERAZINO)-3-PYRIDINAMINE;1-(3-amino-2-pyridyl)-4-methylpiperazine;1-(3-amino-2-pyridyl)-4-methyl-piperazin;2-(4-METHYL-1-PIPERAZINYL)-3-PYRIDINAMINE;2-(4-methyl-piperazin-1-yl)-pyridin-3-ylamine
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CAS No:
2-(4-METHYLPIPERAZINO)-3-PYRIDINAMINE Use and Manufacturing
PREPARATION 24; 2-(4-Methylpiperazin-1-vQpyridin-3-ylamine;. PP26 (0.50 g, 2.25 mmol), ammonium formate (1.00 g, 15.85 mmol) and 10percent Pd on carbon (0.050 g) in MeOH (20 mL) were stirred for 1 h at rt, then filtered (Celite.(TM).) and concentrated. The residue was dissolved in EtOAc and washed with aq. KTo a stirring solution of l-methyl-4-(3-nitro-pyridin-2-yl)-piperazine (LXXXIII) (1.30 g, 5.85 mmol) in MeOH (15 mL) was added 10percent Pd/C. The solution was purged with hydrogen. The solution was stirred at room temperature for 16 h under hydrogen. The solution was filtered through a pad of Celite and concentrated to a residue under vacuum. The residue was purified by column chromatography (100percent CHC1stirring solution of l-methyl-4-(3-nitro-pyridin-2-yl)-piperazine (0543) (LXXXIII) (1.30 g, 5.85 mmol) in MeOH (15 mL) was added 10percent Pd/C. The solution was purged with hydrogen. The solution was stirred at room temperature for 16 h under hydrogen. The solution was filtered through a pad of Celite and concentrated to a residue under vacuum. The residue was purified by column chromatography (100percent CHC → 2:98 MeOH[7N NH
Computed Properties
Molecular Weight:192.26
XLogP3:0.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:192.137496527
Monoisotopic Mass:192.137496527
Topological Polar Surface Area:45.4
Heavy Atom Count:14
Complexity:177
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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2-(4-METHYLPIPERAZINO)-3-PYRIDINAMINE
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