1-Propanamine, 3-chloro-, hydrochloride
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1-Propanamine, 3-chloro-, hydrochloride
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CAS No:
6276-54-6
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Formula:
C3H8ClN.ClH
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Chemical Name:
1-Propanamine, 3-chloro-, hydrochloride
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Synonyms:
1-Propanamine,3-chloro-,hydrochloride;Propylamine,3-chloro-,hydrochloride;3-Amino-1-chloropropane hydrochloride;1-Amino-3-chloropropane hydrochloride;3-Aminopropyl chloride hydrochloride;3-Chloro-1-propanamine hydrochloride;1-Chloro-3-aminopropane hydrochloride;3-Chloropropylamine hydrochloride;109467-93-8
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CAS No:
Description
off-white to yellow-beige crystalline
3-Chloropropylamine Hydrochloride is a building block that has been used as a modifier to N-enrich an activated carbon to increase adsorption. 3-Chloropropylamine Hydrochloride has also been used in as a reactant for the synthesis of cyclic sulfamide derivatives to be used as 11β-Hydroxysteroid Dehydrogenase 1 inhibitors for potential treatment of metabolic syndrome and diabetes.
Characteristics
26
2.07630
Off-white to yellow-beige Crystalline Powder or Chunks
1.004 g/cm3
146-148 °C @ Solvent: Ethanol, Diethyl ether
130.7ºC at 760 mmHg
32.9ºC
Store below +30°C.
Safety Information
3
36/37/38
26-36/37-36-37/39
Xi
Stable under normal temperatures and pressures.
P261, P264, P271, P272, P280, P285, P302+P352, P304+P340, P304+P341, P305+P351+P338, P312, P321, P332+P313, P333+P313, P337+P313, P342+P311, P362, P363, P403+P233, P405, P501
H315
1-Propanamine, 3-chloro-, hydrochloride Use and Manufacturing
To solution of thionyl chloride (8.68 g, 1.32 mmol) in anhydrous chloroform (30 mL) was added dropwise to 3-aminopropan-l-ol (4.49 g, 59.19 mmol) while maintaining the temperature at 0 - 10 °C. The mixture was allowed to warm to room temperature and then heated at reflux for 3 h. The mixture was cooled to room temperature and the precipitate was collected to give 3-chloropropylamine hydrochloride (8A) (7.07 g, 55.15 mmol, 93percent) as a green solid. ESMS m/z 94 (M+H)Step 1: Synthesis of 3-chloropropylamine hydrochloride (8)[00261j To solution of thionyl chloride (8.68 g, 1.32 mmol) in anhydrous chloroform (30 mL) was added dropwise to 3-aminopropan-1-ol (4.49 g, 59.19 mmol) while maintaining the temperature at 0 — 10 °C. The mixture was allowed to warm to room temperature and then heated at reflux for 3 h. The mixture was cooled to room temperature and the precipitate was collected to give 3-chloropropylamine hydrochloride (8) (7.07 g, 55.15 mmol, 93percent) as a green solid. ESMS mlz 94 (M+H).
3-Chloropropylamine hydrochloride was used in chemical treatment of carbon-enriched fly ash concentrates.It was used in the synthesis of linear, star and comb-like polyacrylamides by atomic transfer radical polymerization. It was used in the synthesis of halogen-functionalized aliphatic polyketones (macroinitiators).
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1-Propanamine, 3-chloro-, hydrochloride
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