1,4-BIS(VINYLDIMETHYLSILYL)BENZENE
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1,4-BIS(VINYLDIMETHYLSILYL)BENZENE
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CAS No:
4519-17-9
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Formula:
C14H22Si2
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Chemical Name:
1,4-BIS(VINYLDIMETHYLSILYL)BENZENE
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Synonyms:
1,4-BIS(VINYLDIMETHYLSILYL)BENZENE;1,4-Bis(dimethyl(vinyl)silyl)benzene;[4-[dimethyl(vinyl)silyl]phenyl]-dimethyl-vinyl-silane;ethenyl-[4-[ethenyl(dimethyl)silyl]phenyl]-dimethylsilane;ethenyl-[4-[ethenyl(dimethyl)silyl]phenyl]-dimethyl-silane
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CAS No:
1,4-BIS(VINYLDIMETHYLSILYL)BENZENE Basic Attributes
246.5
246.126007
269580
DTXSID10313370
2931900090
1,4-BIS(VINYLDIMETHYLSILYL)BENZENE Use and Manufacturing
General procedure: Magnesium 1.28 g (52.5 mmol) was added to a dried flask. Then a solution of 6.59 g (25 mmol) 3, 6-(dibromo)benzocyclobutene in 20 mL freshly distilled THF was added dropwise over a period of 2 h. The reaction mixture was heated to 40°C and stirred continuously for 2 h. After cooled to room temperature, a solution of 6.65 g (55 mmol) of (vinyldimethylchloro)silane in 15 mL freshly distilled THF was added into the reaction mixture over a period of 1 h at ambient temperature. The reaction mixture was then heated to 40°C, and stirred for 2 h. Then the mixture was allowed to stand overnight and was poured into distilled water. The aqueous phase was extracted with petroleum ether (30 mL×3). The organic layers were combined and dried over anhydrous sodium sulfate. After removal of the solvents under reduced pressure, the residue was purified by chromatography (petroleum ether) to give 2 of 5.57 g (82percent yield).
Computed Properties
Molecular Weight:246.49
Rotatable Bond Count:4
Exact Mass:246.12600377
Monoisotopic Mass:246.12600377
Heavy Atom Count:16
Complexity:230
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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1,4-BIS(VINYLDIMETHYLSILYL)BENZENE
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