6-Methoxy-2-methylquinoline
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6-Methoxy-2-methylquinoline
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CAS No:
1078-28-0
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Formula:
C11H11NO
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Chemical Name:
6-Methoxy-2-methylquinoline
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Synonyms:
Quinoline,6-methoxy-2-methyl-;Quinaldine,6-methoxy-;6-Methoxy-2-methylquinoline;6-Methoxyquinaldine;2-Methyl-6-methoxyquinoline;NSC 15557
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CAS No:
6-Methoxy-2-methylquinoline Basic Attributes
173.21
173.21
214-080-1
YC360F525A
15557
DTXSID70148246
29334900
Characteristics
22.1
2.6
Beige to gray Fluffy Crystalline Powder
0.973
64-65 °C
138-139 °C @ Press: 5 Torr
47°(117°F)
1.4950 (estimate)
Keep container closed when not in use. Store in a tightly closed container. Store in a cool, dry, well-ventilated area away from incompatible substances.
0.00467mmHg at 25°C
Safety Information
IRRITANT
3
36/37/38
26-37/39-24/25
Xi
Stable under normal temperatures and pressures.
P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, P501
H315
|Warning|H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]|P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, and P501|Aggregated GHS information provided by 44 companies from 3 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.
6-Methoxy-2-methylquinoline Use and Manufacturing
General procedure: The respective 2-methylquinoline (14-20mmol) was dissolved in carbon tetrachloride or benzene (1.3-13.5ml per mmol) and N-bromosuccinimide (1.1 eqv) was added. The mixture was refluxed in the presence of benzoyl peroxide (0.8-1.7mmol) for the indicated below amount of time. After cooling to room temperature, the precipitated succinimide was filtered off and after evaporation af the volatiles under vacuum, the product was purified by flash chromatography.Example 3 Synthesis of 6-methoxy-2-bromomethylquinoline A mixture of EXAMPLE 232 Preparation of 2-(Bromomethyl)-6-methoxyquinoline A solution of 10 g (57.7 mmol) of
Computed Properties
Molecular Weight:173.21
XLogP3:2.6
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:173.084063974
Monoisotopic Mass:173.084063974
Topological Polar Surface Area:22.1
Heavy Atom Count:13
Complexity:172
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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