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6-Methoxyisoquinoline

6-Methoxyisoquinoline structure

CAS No:
52986-70-6
Formula:
C10H9NO
Chemical Name:
6-Methoxyisoquinoline
Synonyms:
6-METHOXY-ISOQUINOLINE;6-Methoxyisoquinoline 90%;6-methoxylisoquinoline;6-Methoxy-2-azanaphthalene;Isoquinoline, 6-methoxy-
Categories:
Pharmaceutical Intermediates > Heterocyclic Compound

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Description

Clear Oil

6-Methoxyisoquinoline Basic Attributes

Molecular Weight：

159.18

Exact Mass：

159.068420

EC Number：

HScode：

2933499090

Characteristics

PSA：

22.1

XLogP3：

2.2

Appearance：

clear oil

Density：

1.1±0.1 g/cm3

Boiling Point：

88-95?C/0.8 Torr

Flash Point：

108.4±10.1 °C

Refractive Index：

1.611

Storage Conditions：

Refrigerator

Safety Information

Marks：

Hazard note：

Irritant

6-Methoxyisoquinoline Use and Manufacturing

The material obtained from Step B (15) was dissolved in CH2CI2 (200 mL) and cooled to O 16 (5.32 g, 33.4 mmol) was slowly added at 0C to cone. H2SO4 (33.5 mL). The mixture was cooled to -25C and NBS (7.68 g, 43.2 mmol) was added at such a rate that the reaction temperature was kept between -25C and -22C. The mixture was stirred at -22C for 2 h and at -18C for 3 h, then poured onto crushed ice. The pH was adjusted to 9 using concentrated aqueous NH3 and the alkaline slurry was then extracted with diethyl ether. The combined organic fractions were washed with 1 N NaOH and water, dried (Na2SO4), filtered and evaporated to dryness to afford 5.65 g (71%) of the target product 17: m/z = 237.8 (M+H)+.A: 5-Bromo-6-hvdroxy-2/-/-isoquinolin-1 -oneTo a solution of A: 5-Bromo-6-hydroxy-2H-isoquinolin-1-one To a solution of (c) Heat a mixture of b) ISOQUINOLIN-6-OL Heat a mixture of Isoquinolin-6-ol Heat a mixture of

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6-Methoxyisoquinoline

CAS No.: 52986-70-6

Content: 99.00%

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