3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE

Step 2: 3-amino-N, N-dimethylbenzenesulfonam ide N, N-Dimethyl-3-nitrobenzenesulfonamide (850 mg, 3.7 mmol) wase dissolved in methanol (20 mL). The wet Pd/C (85 mg) was added to the mixture. The reaction mixture was stirred under hydrogen atmosphere overnight. The catalyst was removed by filtration and the solvent was removed under reduced pressure to give 3-amino-N, Ndimethylbenzenesulfonamide (600 mg, 80percent) as a white solid. LCMS (Method B): 0.48[M+H]= 201.1Prepared analogously to Example 6, 50mg Intermediate 16 and 53mg Prepared analogously to Example 6, prepared starting from 47mg by the Intermediate 14 and 55mg At a bath temperature of 120C, under argon, stirring 150mg Intermediate 10, 192mg

Molecular Weight:200.26
XLogP3:0.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:200.06194880
Monoisotopic Mass:200.06194880
Topological Polar Surface Area:71.8
Heavy Atom Count:13
Complexity:256
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes