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8-Bromoguanine

8-Bromoguanine structure

CAS No:
3066-84-0
Formula:
C5H4BrN5O
Chemical Name:
8-Bromoguanine
Synonyms:
6H-Purin-6-one,2-amino-8-bromo-1,9-dihydro-;Guanine,8-bromo-;6H-Purin-6-one,2-amino-8-bromo-1,7-dihydro-;2-Amino-8-bromo-1,9-dihydro-6H-purin-6-one;8-Bromoguanine;2-Amino-8-bromopurine-6-ol;NSC 7845;2-Amino-8-bromo-6,7-dihydro-1H-purin-6-one;2-Amino-8-bromo-9H-purin-6-ol;2-Amino-8-bromo-1,7-dihydro-purin-6-one;2-Amino-8-bromo-6,9-dihydro-1H-purin-6-one;2-Amino-8-bromo-3,7-dihydropurin-6-one;2-Amino-8-bromo-1H-purin-6(7H)-one;938-83-0
Categories:
Biochemical Engineering > Nucleoside Drugs

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8-Bromoguanine Basic Attributes

Molecular Weight：

230.02

Exact Mass：

230.02

EC Number：

221-320-9

HScode：

2933990090

Characteristics

PSA：

96.2

XLogP3：

0.1

Appearance：

White to off white crystalline powder

Density：

2.82 g/cm3

Boiling Point：

355.3°C at 760 mmHg

Flash Point：

301.1ºC

Refractive Index：

2.087

Storage Conditions：

2-8°C

Safety Information

Packing level：

Ⅲ

Transport codes：

2811

hazard class code：

20/21/22-36/37/38-43-25

safety instructions：

26-36-45-36/37

Marks：

Xn,T

Precautionary statement(s)：

P261, P264, P270, P272, P280, P301+P310, P302+P352, P321, P330, P333+P313, P363, P405, P501

Hazard Statements：

H301

8-Bromoguanine Use and Manufacturing

2-Amino-8- {4-[2-(trifluoromethyl)phenoxy1piperidin- 1 -yl ) - 1 , 9-dihydro-6H-purin-6-one A mixture of 2-amino-8-bromo-l, 9-dihydro-6H-purin-6-one (100 mg, 0.4 mmol), 4-[2- (trifluoromethyl)phenoxy]piperidine (0.24 mL, 0.98 mmol) and triethylamine (0.1 mL, 0.65 mmol) in 2- methoxymethanol/water (4:1, 0.7 mL) was heated at 130 0C for 16 h. The volatiles were evaporated to one third the volume and diluted with saturated aqueous NaHCO3 (2 mL). The resulting solid was filtered and washed with water and then MeOH. The product was dried under high vacuum to give the title product as a solid. lH NMR (500 MHz, DMSO-^): delta 11.26 (s, 1 H), 10.26 (s, 1 H), 7.64-7.60 (m, 2 H), 7.37 (d, 1 H), 7.09 (t, 1 H), 5.97 (s, 1 H), 4.87 (s, 1 H), 3.65 (s, 2 H), 3.50 (s, 2 H), 1.98 (s, 2 H), 1.71 (s, 2 H). MS (+ESI) m/z 395 (MH+).

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2-amino-8-bromo-3,7-dihydropurin-6-one

CAS No.: 3066-84-0

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Guide of 8-Bromoguanine

Basic Attributes
Characteristics
Safety Information
Use and Manufacturing
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8-Bromoguanine

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