3-HYDROXY-4-METHYLPYRIDINE
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3-HYDROXY-4-METHYLPYRIDINE
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CAS No:
1121-19-3
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Formula:
C6H7NO
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Chemical Name:
3-HYDROXY-4-METHYLPYRIDINE
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Synonyms:
3-Hydroxy-4-picoline;4-Methylpyridin-3-ol;4-methyl-3-pyridinol;3-Pyridinol,4-methyl-;3-Hdroxy-4-Methylpyridine;3-HYDROXY-4-METHYLPYRIDINE;3-HYDROXY-4-METHYLPYRIDINE98%;4-Methylpyridin-3-ol,3-Hydroxy-4-picoline
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CAS No:
Characteristics
33.1
0.9
1.120±0.06 g/cm3(Predicted)
118-120 °C
285-290 °C
145.0±22.3 °C
1.551
0.000225mmHg at 25°C
3-HYDROXY-4-METHYLPYRIDINE Use and Manufacturing
To a solution of OH (7.0 g) in methanol (50 ml) was added 3-acetoxy-4-methylpyridine 1 - oxide (51; 1 5.0 g, 106 mmol). The mixture was stirred at room temperature overnight. The methanol was removed under vacuum and the residue was dissolved in water. The solution was neutralized to pH 7 with cone. HC1 and extracted with CHLithium hydroxide monohydrate (32.1 g, 764 mmol) was added to Intermediate 61 (127 g, 841 mmol) in THF (500 mL) and water (500 mL). After 6 h, THF was removed in vacuo, then DCM and 1M aqueous sodium hydroxide solution were added. The layers were separated. The aqueous phase was acidified with concentrated HC1 until the pH was approximately 4-5, then saturated with sodium chloride and extracted with EtOAc. The combined organic layers were washed with brine, dried (Na0.5 mol of 1 mol of
Computed Properties
Molecular Weight:109.13
XLogP3:0.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Exact Mass:109.052763847
Monoisotopic Mass:109.052763847
Topological Polar Surface Area:33.1
Heavy Atom Count:8
Complexity:74.9
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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